Six new benzimidazolyl substituted triaryltriazoles, 3‐(2‐pyridyl)‐4‐(p‐R‐phenyl)‐5‐(2‐benzimidazolyl)‐1,2,4‐triazoles (L1: R = OCH3; L2: R = CH3; L3: R = H; L4: R = Br; L5: R = Cl; L6: R = F) were successfully synthesized. Yield of L1–6 is in the range from 61 to 76%. The compounds L1–6 were characterized by UV–vis, FTIR, 1H‐NMR, ESI‐MS spectra, and elemental analysis. Additionally, the absolute configurations of L1–5 were determined by single crystal X‐ray crystallography.

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