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Graphene oxide (GO) and reduced graphene oxide (RGO) have many outstanding physical and mechanical properties. Uniform and thickness controllable RGO films with large area were prepared by evaporation-induced self-assembly at a liquid/air interface on glass substrates in combination with low temperature thermal reduction at 200 °C. This process has the advantage of good compatibility with flexible and non-flexible substrates. The films are of centimeter scale and their thickness can be controlled. The structural evolution was characterized. The obtained thermal RGO films exhibit excellent optical properties, a high elastic modulus of 76.18 GPa, and a hardness of 6.89 GPa.

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