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In the title complex, [Mn(2)(C(16)H(14)N(2)O(2))(2)(C(2)H(3)O(2))]ClO(4), two [Mn(salen)] moieties [salen is bis(salicylidene)ethylenediamine] are connected through a micro-acetate bridge in a syn-anti fashion. The Mn.Mn distance is 5.365 (1) A.

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The title mononuclear copper(II) compound, [CuCl(C(16)H(22)N(4))]ClO(4), shows a slightly tetrahedrally distorted square-pyramidal coordination with the chlorine ligand at the apical position. The directions of the two N-Me bond axes are syn to the Cu-Cl bond.