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Domino coupling of furan‐2‐yl (phenyl) methanol and 2‐(1H‐pyrrol‐1‐yl) aniline has been achieved in the presence of 10 mol% phosphomolybdic acid in CH3CN under reflux to afford the corresponding biologically active 10‐aryl‐9a,10,12,12a‐tetrahydrobenzo[b]cyclopenta[f]pyrrolo[1,2‐d][1,4]diazepin‐11(9H)‐ones in good yields. Broad substrate scope, short reaction times, environmentally benign, and operational simplicity makes this method more attractive.

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