2014
DOI: 10.1016/j.aoas.2014.11.006
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1H NMR spectral analysis as a new aspect to evaluate the stability of some edible oils

Abstract: Oxidative stability is one of the most important indicators for maintaining the quality of edible oils. 1 H NMR fingerprinting is used to evaluate the stability of edible oils at room temperature. The assignments of the 1 H NMR signals of the major and minor components of unoxidized edible oils and the oil stability prediction were given. Minor components of the oils are playing an essential role in defining oil authenticity and quality. Extra virgin olive oil (EVOO) showed b-sitosterol, whereas, moringa oil (… Show more

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Cited by 40 publications
(17 citation statements)
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“…The oil sample was dissolved in the deuterated chloroform. 1 HNMR spectra of the extracted PSO were recorded using a Bruker DRX‐400 NMR spectrometer (Bruker Instruments) with 1 H nuclei observed at 400 MHz (Almoselhy, Allam, El‐Kalyoubi, & El‐Sharkawy, ).…”
Section: Methodsmentioning
confidence: 99%
“…The oil sample was dissolved in the deuterated chloroform. 1 HNMR spectra of the extracted PSO were recorded using a Bruker DRX‐400 NMR spectrometer (Bruker Instruments) with 1 H nuclei observed at 400 MHz (Almoselhy, Allam, El‐Kalyoubi, & El‐Sharkawy, ).…”
Section: Methodsmentioning
confidence: 99%
“…The oil sample was dissolved in the deuterated chloroform. The 1 H NMR spectra of the extracted PSO were acquired on a Bruker DRX‐400 NMR spectrometer with 1 H nuclei observed at 400 MHz (Bruker International AG, Rheinstetten, Germany) (Almoselhy, Allam, El‐Kalyoubi, & El‐Sharkawy, ).…”
Section: Methodsmentioning
confidence: 99%
“…Signals from 4.40 to 4.70 ppm indicated hydrogen from the glyceryl group [-CH-O-C(¼O)-R]. A doublet at 5.31 ppm with J ¼ 6.24 Hz indicated hydrogens in cis (-CH¼CH-) in the double bonds of the acyl chain [10,[16][17][18][19][20]. A similar 1 H-NMR spectrum was observed for the PGS; however, with hydrogen in trans in the double bonds of the acyl chain [d 5.32; J ¼ 11.73 Hz (Fig.…”
Section: H-nmr Analysesmentioning
confidence: 99%