A Facile and General, One-pot Synthesis of 2-Oxoalkane Phosphonates from Diethylphosphonocarboxylic Acid Chlorides and Organometallic Reagents

Mono and bis[N-aryl(benzyl)]amides of phosphorylacetic acids. One-pot synthesis and extraction of actinides from nitric acid solutions

“…10 Earlier, 11 we have employed the similar procedure for the preparation of N alkyl and N dialkylamides from phosphorylcycloalkanecarboxylic acids with the use of thionyl chloride as the chlorinating agent. Oxalyl chloride 12 (C 6 H 6 , ~20 °C) and sulfuryl chlo ride (CH 2 Cl 2 , ~20 °C) 13 were used for the synthesis of monosubstituted phosphorylacetic acid chlorides. In the latter study, this chlorinating system was demonstrated to be efficient in preparing diethoxyphosphorylacetic acid chloride in nearly quantitative yield.…”

Metabolism-based synthesis, biological evaluation and structure-activity relationship analysis of spirotetramat analogues as potential lipid biosynthesis inhibitors

“…). These analogues were prepared by acylation of compound 4 with acyl chlorides using triethylamine as the acid acceptor . Compound 4 was prepared according to the literature .…”

Synthesis and herbicidal activity of 3‐aryl‐1‐[2‐(aryloxy)propanoyl]imidazolidine‐2,4‐diones

“…All of the solvents and materials were reagent grade and purified as required. 2-(Aryloxy)propanoyl chlorides and 3-aryl-imidazolidine-2,4-diones were prepared according to the methods described in references [12] and [13][14][15][16], respectively.…”