A novel strategy by combining “magnified” matrix solid phase dispersion extraction with high-speed countercurrent chromatography for the rapid and efficient isolation of flavonoids isomers with anti-inflammatory effect from Lindera aggregata (Sims) Kosterm Leaves

Zou, Yanfang; Lv, Yangbin; Peng, Xin; Tong, Shengqiang; Chu, Chu

doi:10.1016/j.scp.2023.101073

Cited by 3 publications

(1 citation statement)

References 29 publications

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“…Four amides (N-p-trans-coumaroyltyramine, aristolactam AII, sauristolactam, and aristolactam BII) were extracted from these samples and determined [21]. Recently, Zou et al [61] proposed a rapid and effective strategy for the isolation of four anti-inflammatory flavonoids from Lindera aggregata (Sims) Kosterm Leaves by combining MSPD with high-speed counter-current chromatography (HSCCC). In that MSPD procedure also, only silica gel was used in the preparation of plant material.…”

Section: Sorbents Used In Mspdmentioning

confidence: 99%

Achievements and Challenges of Matrix Solid-Phase Dispersion Usage in the Extraction of Plants and Food Samples

Zgoła-Grześkowiak,

Grześkowiak,

Ligor

et al. 2024

Processes

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A review of the application of matrix solid-phase dispersion (MSPD) in the extraction of biologically active compounds and impurities from plants and food samples with a particular emphasis on conventional and new types of sorbents has been provided. An overview of MSPD applications for the isolation of organic residues from biological samples, determined using chromatographic and spectroscopic techniques, has been presented. In this study, procedural solutions that may extend MSDP applicability for the extraction such as vortex-assisted, ultrasound-assisted, microwave-assisted, and extraction with a magnetic sorbent have been discussed. Special attention has been paid to MSPD sorbents including modified silica, diatomite, magnesium silicate, alumina, carbon materials (carbon nanotubes, graphene oxide, graphene, or graphite), molecularly imprinted polymers, and cyclodextrin. An important aspect of the MSPD procedure is the use of high-purity and environmentally friendly solvents for extraction (e.g., deep eutectic solvents), with such criteria being the most important for modern analytical chemistry. Many advantages of MSPD are presented, such as high recoveries, the requirement for a smaller volume of solvent, and shorter procedure times than classical methods.

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Section: Sorbents Used In Mspdmentioning

confidence: 99%