2023
DOI: 10.1080/00397911.2023.2211772
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A practical total synthesis of wedelolactone

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Cited by 3 publications
(3 citation statements)
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“…The aldehydes 53-55, 57, 58, 61, 62, and 65-67 were previously obtained in our laboratory [48]. The 2,4,5-trihydroxybenzaldehyde (60) was obtained by formylation of 1,2,4-trihydroxybenzene (70) with triethyl orthoformate mediated by AlCl 3 in toluene [66].…”
Section: Syntheses and Characterizationmentioning
confidence: 99%
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“…The aldehydes 53-55, 57, 58, 61, 62, and 65-67 were previously obtained in our laboratory [48]. The 2,4,5-trihydroxybenzaldehyde (60) was obtained by formylation of 1,2,4-trihydroxybenzene (70) with triethyl orthoformate mediated by AlCl 3 in toluene [66].…”
Section: Syntheses and Characterizationmentioning
confidence: 99%
“…Absorption maxima are reported in wavenumbers (cm -1 ). 1 H-NMR and 13 C-NMR spectra were recorded on Jeol 400yh (Tokyo, Japan) (399.78 MHz for 1 H and 100.52 MHz for 13 The literature procedure was adapted for the preparation of hydrazide-hydrazones 1-3, 5-11, 14-25, 27-30 [48], 32 [71], 31, and 33-35 [47]; hydrazides 38-40 [47]; aldehydes 53-55, 58, 61, 62 [48,89], 60 [66], 63 [67], 65 [48,90], 66, 67 [48], and 68 [69]; and phenol 72 [68].…”
Section: Reagents and Materialsmentioning
confidence: 99%
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