A SPE-LC-MS/MS Method for the Detection of Low Concentrations of Pharmaceuticals in Industrial Waste Streams

Deegan, Ann-Marie; Cullen, Mark R.; Oelgemöller, Michael; Nolan, Kieran; Tobin, John M.; Morrissey, Anne

doi:10.1080/00032719.2011.565444

Cited by 4 publications

(1 citation statement)

References 31 publications

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“…Literature survey reveals that quantification of solifenacin in human plasma [11,12], rat plasma [13], pharmaceutical compounds [14][15][16][17], and industrial waste streams [18] was reported. These methods were reported by using LC-MS/MS [11,12,18], HPLC [13][14][15][16], and HPTLC [17]. Among all, quantification of solifenacin by LC-MS/MS in biological matrices [11][12][13] was proved best results.…”

Section: Introductionmentioning

confidence: 99%

Analytical Method Development and Validation of Solifenacin in Pharmaceutical Dosage Forms by RP-HPLC

Shaik

Puttagunta

Bannoth

et al. 2014

ISRN Analytical Chemistry

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A new, accurate, precise, and robust HPLC method was developed and validated for the determination of solifenacin in tablet dosage form. The chromatographic separation was achieved on an Inertsil ODS 3V C18 (150 mm × 4.6 mm, 5 μm) stationary phase maintained at ambient temperature with a mobile phase combination of monobasic potassium phosphate (pH 3.5) containing 0.1% triethylamine and methanol (gradient mode) at a flow rate of 1.5 mL/min, and the detection was carried out by using UV detector at 220 nm. The performance of the method was validated according to the present ICH guidelines.

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Section: Introductionmentioning

confidence: 99%

Analytical Method Development and Validation of Solifenacin in Pharmaceutical Dosage Forms by RP-HPLC

Shaik

Puttagunta

Bannoth

et al. 2014

ISRN Analytical Chemistry

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Crystal plane directed interaction of TiO2 [1 0 1] with AgNPs [1 1 1] silver nanoparticles enhancing solar light induced photo-catalytic oxidation of ciprofloxacin: Experimental and theoretical studies

Huerta-Aguilar

Gutiérrez

Thangarasu

2020

Chemical Engineering Journal

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Bioanalytical method for quantification of Solifenacin in rat plasma by LC-MS/MS and its application to pharmacokinetic study

et al. 2014

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Background: Solifenacin succinate is a competitive muscarinic acetylcholine receptor antagonist used in the treatment of overactive bladder with or without urge incontinence. Methods: Liquid chromatography-tandem mass spectrometry method was used for quantification of Solifenacin (SF) in rat plasma. Solifenacin-d5 (SFD5) used as an internal standard. Chromatographic separation was performed Gemini-NX C18, 50 × 4. Conclusions: This method is successfully applied in the Pharmacokinetic study of rat plasma.

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A SPE-LC-MS/MS Method for the Detection of Low Concentrations of Pharmaceuticals in Industrial Waste Streams

Cited by 4 publications

References 31 publications

Analytical Method Development and Validation of Solifenacin in Pharmaceutical Dosage Forms by RP-HPLC

Analytical Method Development and Validation of Solifenacin in Pharmaceutical Dosage Forms by RP-HPLC

Crystal plane directed interaction of TiO2 [1 0 1] with AgNPs [1 1 1] silver nanoparticles enhancing solar light induced photo-catalytic oxidation of ciprofloxacin: Experimental and theoretical studies

Bioanalytical method for quantification of Solifenacin in rat plasma by LC-MS/MS and its application to pharmacokinetic study

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