A study of dried mandarin (
            <i>Clementina orogrande</i>
            ) peel applying supercritical carbon dioxide using co‐solvent: Influence on oil extraction, phenolic compounds, and antioxidant activity

Quispe‐Fuentes, Issis; Uribe, Elsa; López, Jéssica; Contreras, Daniella; Poblete, Jacqueline

doi:10.1111/jfpp.16116

Cited by 14 publications

(6 citation statements)

References 37 publications

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“…Figure 10 shows that the higher pressures and lowest particle size increased the solubility of the extract because the increase in pressure enhances the density of solvents. In addition, the increase in pressure increases the solvation power of the ScCO 2 mixture to roselle 32 . Table 4 also shows that the lowest particle size of 250 µm < dp < 355 µm gives the highest solubility TAC, TPC and TFC.…”

Section: Resultsmentioning

confidence: 99%

Influence of particle size in supercritical carbon dioxide extraction of roselle (Hibiscus sabdariffa) on bioactive compound recovery, extraction rate, diffusivity, and solubility

Putra

Rizkiyah

Aziz

et al. 2023

Sci Rep

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The purpose of this work was to establish the best particle size for recovering high yields of total phenolic compounds (TPC), total anthocyanin compounds(TAC) and total flavonoid compounds (TFC) from roselle (Hibiscus sabdariffa) by applying supercritical carbon dioxide (ScCO2). The extraction rate, diffusivity and solubility of yield in ScCO2 were also studied and calculated utilizing models. Pressure (10 and 30 MPa), temperature (40 and 60 °C), and particle size (250 µm < dp < 355 µm, 355 µm < dp < 425 µm and 425 µm < dp < 500 µm) were employed as variables in this experiment. The greatest recovery was 11.96% yield, 7.16 mg/100 g TAC, 42.93 mg/100 g TPC and 239.36 mg/100 g TFC under the conditions of 30 MPA, 40 °C and 250 µm < dp < 355 µm, respectively. The extraction rate of supercritical carbon dioxide in roselle extraction ranged from 5.19 E−03 to 1.35 E−03 mg/s fitted using the Esquivel model. The diffusivity coefficient of ScCO2 ranged from 2.17E−12 to 3.72E−11 mg/s2, as fitted by a single sphere model. The greatest solubility of global yield, TAC, TPC and TFC in ScCO2 was 1.50 g/L, 0.3 mg/L, 1.69 mg/L and 9.97 mg/L, respectively, with a particle size of 250 µm < dp < 355 µm. The smaller particle size of roselle provides the maximum bioactive compound recovery and solubility. Furthermore, the diffusivity and extraction of ScCO2 are increased by decreasing the particle size. Therefore, a smaller particle size is appropriate for roselle extraction by ScCO2 based on the experimental and modelling data.

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Section: Resultsmentioning

confidence: 99%

Influence of particle size in supercritical carbon dioxide extraction of roselle (Hibiscus sabdariffa) on bioactive compound recovery, extraction rate, diffusivity, and solubility

Putra

Rizkiyah

Aziz

et al. 2023

Sci Rep

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“…The quality of natural extracts is significantly related to the extraction method, solvents used, vegetal matrix characteristics, and storage conditions. The selection of solvents must be carefully selected to maximize the yield and selectivity [ 29 , 60 , 61 ].…”

Section: Conventional Extraction Of Anthocyaninsmentioning

confidence: 99%

Insight into Green Extraction for Roselle as a Source of Natural Red Pigments: A Review

et al. 2023

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Roselle (Hibiscus sabdariffa L.) is a source of anthocyanins as red pigments that is extensively farmed in tropical and subtropical regions, including Indonesia, Malaysia, China, Thailand, Egypt, Mexico, and West India. The roselle plant contains a variety of nutrients, including anthocyanins, organic acids, pectin, etc. Due to the toxicity and combustibility of the solvents, traditional extraction methods for these compounds are restricted. Obtaining pure extracts is typically a lengthy procedure requiring many processes. Supercritical carbon dioxide (ScCO2) extraction as a green technology is rapidly improving and extending its application domains. The advantages of this method are zero waste production, quicker extraction times, and reduced solvent consumption. The ScCO2 extraction of natural pigments has great promise in food, pharmaceuticals, cosmetics, and textiles, among other uses. The ScCO2 technique for natural pigments may also be advantageous in a variety of other contexts. Due to their minimal environmental risk, the high-quality red pigments of roselle rich in anthocyanins extracted using ScCO2 extraction have a high sustainability potential. Therefore, the objective of this review is to increase knowledge related to the natural colorant of roselle as a substitute for chemically manufactured colorants using ScCO2 as a green method. This article covers ScCO2 extraction, particularly as it relates to the optimization of pigments that promote health. This article focuses on the high extraction efficiency of ScCO2 extraction. Natural colorants extracted via ScCO2 are regarded as safe compounds, especially for human consumption, such as novel functional food additives and textile and pharmaceutical colors.

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“…The supercritical fluid extraction of polar compounds, in general, is conducted using an organic solvent as the modifier (frequently ethanol). For example, bioactive compounds are extracted from mandarin peel [175] using scCO 2+ 5 and 10% ethanol, from papaya [176] seeds using scCO 2+ 2-8% ethanol, from walnut husk [177] using scCO 2+ 20% ethanol, or from olive residues [178] (leaves, pomace and prunings) using scCO 2+ 60% ethanol. The results in terms of total phenolic compounds and antioxidant activity were, in some cases, compared to the ones obtained through conventional extraction: when phenolic antioxidants were extracted from papaya agro-industrial waste, the yield in the ethanolic extract was slightly higher than the one in the scCO 2+ ethanol extract, but the latter had higher antioxidant activity in vegetable edible oil [176].…”

Section: Combined Extractionsmentioning

confidence: 99%

High-Pressure Technologies for the Recovery of Bioactive Molecules from Agro-Industrial Waste

Pettinato

Campardelli

et al. 2022

Applied Sciences

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Large amounts of food waste are produced each year. These residues require appropriate management to reduce their environmental impact and, at the same time, economic loss. However, this waste is still rich in compounds (e.g., colorants, antioxidants, polyphenols, fatty acids, vitamins, and proteins) that can find potential applications in food, pharmaceutical, and cosmetic industries. Conventional extraction techniques suffer some drawbacks when applied to the exploitation of food residues, including large amounts of polluting solvents, increased time of extraction, possible degradation of the active molecules during extraction, low yields, and reduced extraction selectivity. For these reasons, advanced extraction techniques have emerged in order to obtain efficient residue exploitation using more sustainable processes. In particular, performing extraction under high-pressure conditions, such as supercritical fluids and pressurized liquid extraction, offers several advantages for the extraction of bioactive molecules. These include the reduced use of toxic solvents, reduced extraction time, high selectivity, and the possibility of being applied in combination in a cascade of progressive extractions. In this review, an overview of high-pressure extraction techniques related to the recovery of high added value compounds from waste generated in food industries is presented and a critical discussion of the advantages and disadvantages of each process is reported. Furthermore, the possibility of combined multi-stage extractions, as well as economic and environmental aspects, are discussed in order to provide a complete overview of the topic.

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A study of dried mandarin ( Clementina orogrande ) peel applying supercritical carbon dioxide using co‐solvent: Influence on oil extraction, phenolic compounds, and antioxidant activity

Cited by 14 publications

References 37 publications

Influence of particle size in supercritical carbon dioxide extraction of roselle (Hibiscus sabdariffa) on bioactive compound recovery, extraction rate, diffusivity, and solubility

Influence of particle size in supercritical carbon dioxide extraction of roselle (Hibiscus sabdariffa) on bioactive compound recovery, extraction rate, diffusivity, and solubility

Insight into Green Extraction for Roselle as a Source of Natural Red Pigments: A Review

High-Pressure Technologies for the Recovery of Bioactive Molecules from Agro-Industrial Waste

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