A versatile approach for the preparation of matrix-matched standards for LA-ICP-MS analysis – Standard addition by the spraying of liquid standards

Willner, Jakob; Brunnbauer, Lukas; Larisegger, Silvia; Nelhiebel, Michael; Marchetti‐Deschmann, Martina; Limbeck, Andreas

doi:10.1016/j.talanta.2023.124305

Cited by 6 publications

(6 citation statements)

References 34 publications

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“…12,31,55,56,66,79 The best reported detection limits for sulfur using ICP-QMS were approximately 0.1-0.3 ng/g, which were achieved with the assistance of a desolvation device or LA. 30,111 Such low detection limits can be attributed to the suppressed 16 O2 + interferences due to the dry plasma condition.…”

Section: Measurands and Isotopes For Sulfur Analysis Using Icp-msmentioning

confidence: 99%

“…LA-ICP-QMS was used to determine the concentration of sulfur (or used as internal standard) in pea seedlings, pyrite, chalcopyrite, sphalerite, sulfides, magmatichydrothermal fluid, glass, minerals, melt inclusions, black shale, human skin, and thin-films. 19,23,35,38,43,66,74,84,90,111 The relatively higher concentrations of sulfur in the samples allowed for sulfur to be analyzed by the measurement of 34 S + . 23,74,90 The dry plasma conditions in LA-ICP-QMS suppressed the formation of 16 O2 + interferences and allowed the analysis of sulfur by measuring 32 S + .…”

Section: La-icp-ms For the Determination Of The Sulfur Concentration ...mentioning

confidence: 99%

“…23,74,90 The dry plasma conditions in LA-ICP-QMS suppressed the formation of 16 O2 + interferences and allowed the analysis of sulfur by measuring 32 S + . 43,66,111 LA-HR-ICP-MS was used to determine the sulfur content in human serum, fluid inclusions, copper, and copper alloys. 9,37,44,85 Transferrin and albumin human serum were quantified by using ID-LA-HR-ICP-MS to measure the sulfur content after polyacrylamide gel electrophoresis separation, which provided a high precision analysis with a low relative uncertainty (~1.5-3%).…”

Section: La-icp-ms For the Determination Of The Sulfur Concentration ...mentioning

confidence: 99%

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Review: Sulfur Analysis using Inductively Coupled Plasma Mass Spectrometry

Zhu

2023

At.Spectrosc.

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This paper reviews the use of inductively coupled plasma mass spectrometry (ICP-MS) for sulfur analyses, covering articles published between January 2015 and April 2023. The ICP-MS instruments reported in the articles were classified as quadrupole ICP-MS, tandem quadrupole ICP-MS, high resolution ICP-MS, and multi-collector ICP-MS, each accounting for over 20% of the articles. Each type of ICP-MS instrument achieved detection limits < 1.0 ng/g. Laser ablation and chromatography hyphenated ICP-MS accounted for > 30% of the articles, with special attention paid to direct/imaging and speciation analyses. The leading research field in sulfur analysis is geology, followed by biology, environment, food/feed, and energy. Determination of sulfur concentrations, chemical speciation analysis of sulfur compounds, and sulfur isotope analysis accounted for approximately 30-40% of the articles. The most frequently measured sulfur isotope was 32 S, followed by 34 S and 33 S, whereas one article reported the measurement of 36 S. Selected topics of sulfur analysis using ICP-MS in research fields, hyphenated instruments, and typical applications are also introduced.www.at-spectrosc.com/as/article/pdf/2023187

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Section: Measurands and Isotopes For Sulfur Analysis Using Icp-msmentioning

confidence: 99%

Section: La-icp-ms For the Determination Of The Sulfur Concentration ...mentioning

confidence: 99%

Section: La-icp-ms For the Determination Of The Sulfur Concentration ...mentioning

confidence: 99%

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Review: Sulfur Analysis using Inductively Coupled Plasma Mass Spectrometry

Zhu

2023

At.Spectrosc.

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“…LA-ICP-MS has gained popularity in many different fields, like biology, 1,2 geology, 3,4 and material science, 5,6 for the analysis of solid samples, due to its high dynamic range, low limits of detections, and high sample throughput. 7,8 Moreover, LA-ICP-MS is commonly used for imaging and depth profiling experiments.…”

Section: Introductionmentioning

confidence: 99%

Quantitative depth profile analysis using short single pulse responses in LA-ICP-Q-MS experiments

Podsednik,

Fahrnberger,

Gibbs

et al. 2024

J. Anal. At. Spectrom.

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“…One final paper of interest that is potentially applicable to several different sample types was presented by Willner et al 11 It is well known that LA-ICP-MS can be problematic with regard to calibration since certified materials that are extremely closely matched in terms of matrix composition, hardness, density, boiling point, etc. are needed.…”

Section: Introductionmentioning

confidence: 99%