Additions and Corrections - Synthesis of Sugar-Like Phosphates by the Oxyphosphorane Condensation. Reaction of Glyoxal with Trialkyl Phosphites and Preparation of Phosphate Esters of Glycoaldehyde, α-Hydroxy β-Keto Aldehydes, and Hydroxymalonaldehyde Chloride.

Ramírez, Fausto; Glaser, Stephen L.; Bigler, Allan J.; Pilot, J. F.

doi:10.1021/ja01048a605

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1976

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“…26 The carbon atom, C(20), and three surrounding oxygen atoms of the carbonate group are planar, with deviations from the least-squares plane of 0.001 Á. The angles around C (20) vary from 106.9°to 127.2°even though the suni is 360°. This represents a considerable distortion from the normal 120°in the carbonate ion.27 Inorganic Carbonates show some variations from 120°, but not as large as these.…”

Section: Discussionmentioning

confidence: 99%