An effective room temperature nuclear iodination of aromatic compounds using molecular iodine and ammonium acetate

Gopireddy, Sreenivasulu Reddy; Sebastian, Sharol; Gupta, Manoj K.; Kumar, Deepak; Chandrasekhar, Kothapalli Bannoth

doi:10.1007/s00706-023-03084-1

Monatsh Chem

2023

DOI: 10.1007/s00706-023-03084-1

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An effective room temperature nuclear iodination of aromatic compounds using molecular iodine and ammonium acetate

Sreenivasulu Reddy Gopireddy,

Sharol Sebastian,

Manoj K. Gupta

et al.

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2025

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Cited by 2 publications

References 76 publications

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Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions

Peglow,

Thomaz,

Nobre

et al. 2024

Chemistry An Asian Journal

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This manuscript reports a novel method for the direct iodination of the C‐4 pyrazole ring generated in situ by the reaction of 1,1,3,3‐tetramethoxypropane and various hydrazines. In this approach, potassium iodate (KIO3) and (PhSe)2 are used as catalysts under acidic conditions. This protocol provides a convenient method for the efficient synthesis of 4‐iodo‐1‐aryl‐1H‐pyrazoles, valuable intermediates for several different coupling reactions.

show abstract

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions

Peglow,

Thomaz,

Nobre

et al. 2024

Chemistry An Asian Journal

View full text Add to dashboard Cite

show abstract

Recent advances in the electrophilic halogenation of aromatic compounds using N-halosuccinimides (NXS)

Tanemura

2025

Tetrahedron Letters

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An effective room temperature nuclear iodination of aromatic compounds using molecular iodine and ammonium acetate

Cited by 2 publications

References 76 publications

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions

Recent advances in the electrophilic halogenation of aromatic compounds using N-halosuccinimides (NXS)

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An effective room temperature nuclear iodination of aromatic compounds using molecular iodine and ammonium acetate

Cited by 2 publications

References 76 publications

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO3/PhSeSePh System under Acidic Conditions

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO3/PhSeSePh System under Acidic Conditions

Recent advances in the electrophilic halogenation of aromatic compounds using N-halosuccinimides (NXS)

Contact Info

Product

Resources

About

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions

Efficient Synthesis and Iodine‐Functionalization of Pyrazoles via KIO₃/PhSeSePh System under Acidic Conditions