2006
DOI: 10.1080/15533170600910694
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An Interesting Array of Cyclic Tetramer Water in the Molecular Structure of [V6O12(phen)4(CH3O)4] · 4H2O

Abstract: A hydrothermal reaction of a mixture of Eu 2 O 3 , V 2 O 5 , 4,4 0 -bpy, phen, HCl and ethylenediamine in methanol solution resulted in the unexpected complex, [V 6 O 12 (phen) 4 (CH 3 O) 4 ] . 4H 2 O, which was then characterized by single-crystal X-ray diffraction. This complex crystallizes in the triclinic system with the space group P-1 and cell parameters a 5 9.778(4) Å , b 5 11.620(5) Å , c 5 13.271(5) Å , a 5 73.433(8)8 8 8 8 8, b 5 77.068 (8)8 8 8 8 8, g 5 87.509(8)8 8 8 8 8, and Z52 with R 1 5 0.0726.… Show more

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Cited by 7 publications
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