Analysis of Th and U in thorium-based mixed-oxide fuel using wavelength dispersive X-ray fluorescence spectrometer

Pandey, Ashok K.; Dhara, Sangita; Khan, Fahmida; Kelkar, Anoop; Kumar, Pradeep; Bhatt, Ranu; Behere, P.G.

doi:10.1007/s10967-018-6387-y

Cited by 7 publications

(4 citation statements)

References 26 publications

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“…10,11 There are some reports in the literature where these EDXRF and WDXRF techniques have been utilized for the compositional analysis of MOX fuel pellets. 9,12–14 However, these techniques require matrix-matched calibration standards due to the presence of severe matrix effects in XRF geometry. The calibration process itself is time-consuming.…”

Section: Introductionmentioning

confidence: 99%

“…4 Moreover, the (Th, U)O 2 -based MOX fuel can produce two daughter products, e.g., 212 Bi and 208 Tl, which emit high energy gamma radiation. 9 This makes handling of these types of fuel pellets extremely difficult. So, due to all of these above mentioned difficulties, it is extremely important to develop a green analytical methodology for direct, fast, non-destructive analysis, which does not require any corrosive acids, like HNO 3 and HF.…”

Section: Introductionmentioning

confidence: 99%

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A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration

Kanrar

Sanyal

Pai

2022

J. Anal. At. Spectrom.

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Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration

Kanrar

Sanyal

Pai

2022

J. Anal. At. Spectrom.

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“…Pandey et al 54,55 determined the Th and U composition in thorium-based ThO 2 -UO 2 mixed-oxide fuel using a benchtop sequential WD-XRF SuperMini spectrometer (Rigaku Corporation, Japan). The instrument was equipped with a low power 200 W Pd tube, which had a maximum voltage of 50 kV, 3 different collimators, 3 analyzer crystals and a FPC and SC detector.…”

Section: Commercially Available Wd-xrf Instruments and Applicationsmentioning

confidence: 99%

A review of laboratory, commercially available, and facility based wavelength dispersive X-ray fluorescence spectrometers

De Pauw,

Tack,

Vincze

2024

J. Anal. At. Spectrom.

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“…Sampel berikutnya diiradiasi sinar X (terjadi pancaran elektron (fluoresensi) dengan atmosfer gas helium, menggunakan spektrum panjang gelombang dengan intensitas. Pancaran elektron akan ditangkap oleh detektor, sehingga dapat dideteksi unsur mineral (salah satunya Fe) yang terdapat pada sorbet (Pandey et al, 2019).…”

Section: Prosedur Analisis Kadar Zat Besi Dengan Metode Xrfunclassified

Tingkat Penerimaan, Kadar Zat Besi dan Vitamin C Sorbet Berbahan Daun Kelor dan Jambu Biji Merah untuk Anemia Defisiensi Besi (Level of Acceptance, Iron and Vitamin C Content of Moringa Leaves and Red Guava Sorbet for Iron Deficiency Anemia)

Arviyani

Afifah

Noer

et al. 2021

J. Apl. Teknol. Pang.

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AbstrakPenelitian ini bertujuan menganalisis tingkat penerimaan, kadar zat besi dan vitamin C sorbet berbahan daun kelor dan jambu biji merah. Anemia defisiensi besi merupakan penurunan simpanan zat besi karena kehilangan zat besi tubuh (perdarahan, infeksi, gangguan penyerapan zat besi, dan kondisi peningkatan kebutuhan zat besi), yang mengakibatkan suplai zat besi tidak mencukupi untuk produksi sel darah merah (eritropoiesis). Anemia defisiensi besi dapat mengakibatkan penurunan daya tahan tubuh dan produktivitas. Pengembangan produk pangan dapat dilakukan sebagai upaya penanggulangan anemia defisiensi besi, dengan menggabungkan pangan sumber zat besi non-haem dengan pangan sumber vitamin C. Sorbet berbahan daun kelor dan jambu biji merah dapat dimanfaatkan sebagai alternatif snack berbasis pangan fungsional untuk mengatasi anemia defisiensi besi. Penelitian dilakukan 2 tahap, yaitu penelitian pendahuluan berupa uji tingkat penerimaan dengan metode hedonik pada 34 panelis. Formula yang diujikan meliputi, sorbet pengenceran 50 mL (formula 1), 100 mL (formula 2), dan 150 mL (formula 3). Tahap selanjutnya, formula terpilih dengan skor hedonik tertinggi dianalisis kadar zat besi dengan metode XRF dan vitamin C dengan metode HPLC. Formula terbaik berdasarkan uji tingkat penerimaan adalah sorbet dengan pengenceran 100 mL (formula 2). Sorbet formula 2 memiliki rerata kadar zat besi sebesar 0,3 mg/100 g dan vitamin C sebesar 80,17 mg/100 g. Sorbet formula 2 memberikan kontribusi zat besi terhadap AKG remaja putri usia 13-15 dan 16-18 tahun sebesar 2%. Sorbet formula 2 memberikan kontribusi vitamin C terhadap AKG remaja putri usia 13-15 dan 16-18 tahun masing-masing sebesar 123,3% dan 106,9%. AbstractThis study was aimed to analyze the level of acceptance, iron and vitamin C sorbet content made from moringa leaves and red guava. Iron deficiency anemia was a condition of decreased in iron stores due to loss of body iron (bleeding, infection, impaired iron absorption, and increased iron demand conditions) that resulted in insufficient iron supply for red blood cell production (erythropoiesis). Iron deficiency anemia could result in decreased endurance and productivity. One of the efforts to deal with iron deficiency anemia was the development of food products. Food product development could be done by combining non-haem iron source food with vitamin C source food. Sorbet made from moringa leaves and red guava could be used as an alternative to a functional food-based snack to treat iron deficiency anemia. The study were conducted in 2 stages, preliminary study in the form of a hedonic test on 34 panelists to analyze level of acceptance. The formulas tested included, sorbet with a dilution of 50 mL (formula 1), 100 mL (formula 2), and 150 mL (formula 3). The next step, one formula was selected with the highest hedonic score analyzed the iron content by the XRF method and the vitamin C content by the HPLC method. The best formulation based on the level of acceptance test must be sorbet with 100 mL dilution (formula 2). Iron content averages of formula 2 must be 0.3mg/100 g and vitamin C content averages must be 80.17mg/100 g. Formula 2 contribute to iron based on adolescents girl’s AKG (13-15 and 16-18 years old) was 2%, vitamin C based on adolescents girl’s AKG (13-15 and 16-18 years old) were 123.3% and 106.9% respectively.

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Analysis of Th and U in thorium-based mixed-oxide fuel using wavelength dispersive X-ray fluorescence spectrometer

Cited by 7 publications

References 26 publications

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration

A review of laboratory, commercially available, and facility based wavelength dispersive X-ray fluorescence spectrometers

Tingkat Penerimaan, Kadar Zat Besi dan Vitamin C Sorbet Berbahan Daun Kelor dan Jambu Biji Merah untuk Anemia Defisiensi Besi (Level of Acceptance, Iron and Vitamin C Content of Moringa Leaves and Red Guava Sorbet for Iron Deficiency Anemia)

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Analysis of Th and U in thorium-based mixed-oxide fuel using wavelength dispersive X-ray fluorescence spectrometer

Cited by 7 publications

References 26 publications

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O2 fuel pellets by the X-Ray Fluorescence technique using single universal calibration

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O2 fuel pellets by the X-Ray Fluorescence technique using single universal calibration

A review of laboratory, commercially available, and facility based wavelength dispersive X-ray fluorescence spectrometers

Tingkat Penerimaan, Kadar Zat Besi dan Vitamin C Sorbet Berbahan Daun Kelor dan Jambu Biji Merah untuk Anemia Defisiensi Besi (Level of Acceptance, Iron and Vitamin C Content of Moringa Leaves and Red Guava Sorbet for Iron Deficiency Anemia)

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Product

Resources

About

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration

A green analytical approach for the direct non-destructive compositional analysis of (Th, U)O₂ fuel pellets by the X-Ray Fluorescence technique using single universal calibration