A new series of metal Complexes were prepared by refluxing nickel chloride with hot methanolic solution mixture of 8-Hydroxyquinoline and Schiff bases(L1-L6). Schiff base ligands were synthesised by the condensation of 4-aminopheno, 4-aminosalicylic acid, 2-aminobenzthiazole with salicylaldehyde and vanillin. The metal complexes have been characterised by gravimetric metal analysis, magnetic moment,conductivity measurement, 1HNMR and IR analysis.