Bio-inspired low elastic biodegradable Mg-Zn-Mn-Si-HA alloy fabricated by spark plasma sintering

Prakash, Chander; Singh, Sunpreet; Pabla, B. S.; Sidhu, Sarbjeet Singh; Uddin, Md. Sharif

doi:10.1080/10426914.2018.1512117

Cited by 76 publications

(29 citation statements)

References 59 publications

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“…The high value of sintering pressure induces the high driving force, which helps in densifying or compacting the powder particles. Reportedly elevated sintering temperature assists the coalescence of the powder and reduces the porosity [ 30 , 31 ]. Figure 4 a presents the sintering of powder particles during the SPS process.…”

Section: Resultsmentioning

confidence: 99%

“…Therefore, the possible reaction behind the appearance of O element in the as-fabricated alloys resulted from handling of powder sample after milling and before sintering. The uniformly distributed HA in the composite leads to increase in the corrosion resistance [ 29 , 30 , 31 ]. On the other hand, when Si was used as an alloying element instead of HA, the typical change in the structure has been witnessed.…”

Section: Resultsmentioning

confidence: 99%

“…Then, the blended powder was consolidated by the SPS process (SPS-5000 machine; model: Dr. Sinter SPS-625, Fuji Electronic Industrial Co. Ltd., Tsurugashima, Japan). The SPS was carried out at a heating rate of 50 °C /min (for a holding time of 5 min), under vacuum, and at different sintering temperatures and pressure conditions as illustrated in Table 2 , as per the procedure reported elsewhere [ 29 , 30 , 31 ]. Figure 1 presents the fabrication route for the synthesis of Mg–Zn–Mn–(HA–Si) alloy.…”

Section: Methodsmentioning

confidence: 99%

“…The simulated body fluid (SBF) test was conducted to find out the degradation rate of the specimens after 3, 7, and 14 days. The samples were well polished and dipped into the SBF solution in sterilized vials as per the ASTM-G31-72 standard, as reported in [ 31 , 37 ]. After a predetermined time period of immersion, the samples were retrieved from the glass vial, cleaned by water, and dehydrated into the desiccators for 24 h. The degradation rate was determined by the weight loss due to Mg 2+ ion release in the SBF solution.…”

Section: Methodsmentioning

confidence: 99%

“…The alloying of HA (5 wt %) improves the corrosion resistance of Mg [ 29 , 30 ]. Further, Prakash et al [ 31 ] investigated the effect of mechanical alloying-assisted SPS process (MA-SPS) parameters on structural porosity, elastic modulus, and hardness of the composite. Multi-objective particle swarm optimization (MO-PSO) has been utilized to determine the optimal setting of MA-SPS to sinter mechanically tuned biocompatible composites with improved corrosion properties.…”

Section: Introductionmentioning

confidence: 99%

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Synthesis, Characterization, Corrosion Resistance and In-Vitro Bioactivity Behavior of Biodegradable Mg–Zn–Mn–(Si–HA) Composite for Orthopaedic Applications

et al. 2018

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Recently, magnesium (Mg) has gained attention as a potential material for orthopedics devices, owing to the combination of its biodegradability and similar mechanical characteristics to those of bones. However, the rapid decay rate of Mg alloy is one of the critical barriers amongst its widespread applications that have provided numerous research scopes to the scientists. In this present, porous Mg-based biodegradable structures have been fabricated through the hybridization of elemental alloying and spark plasma sintering technology. As key alloying elements, the suitable proportions of silicon (Si) and hydroxyapatite (HA) are used to enhance the mechanical, chemical, and geometrical features. It has been found that the addition of HA and Si element results in higher degree of structural porosity with low elastic modulus and hardness of the Mg–Zn–Mn matrix, respectively. Further, addition of both HA and Si elements has refined the grain structure and improved the hardness of the as-fabricated structures. Moreover, the characterization results validate the formation of various biocompatible phases, which enhances the corrosion performance and biomechanical integrity. Moreover, the fabricated composites show an excellent bioactivity and offer a channel/interface to MG-63 cells for attachment, proliferation and differentiation. The overall results of the present study advocate the usefulness of developed structures for orthopedics applications.

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Section: Resultsmentioning

confidence: 99%

Section: Resultsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

See 3 more Smart Citations

Synthesis, Characterization, Corrosion Resistance and In-Vitro Bioactivity Behavior of Biodegradable Mg–Zn–Mn–(Si–HA) Composite for Orthopaedic Applications

et al. 2018

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Enhancing Microstructural, Thermal, Mechanical, and Corrosion Response of a Bio/Eco‐Compatible Mg–2Zn–1Ca–0.3Mn Alloy Using Two Types of Cryogenic Treatments

Sole,

Johanes,

Gupta

2024

Adv Eng Mater

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Biocompatible Mg–2Zn–1Ca–0.3Mn is synthesized using the disintegrated metal deposition process and subjected to two types of cryogenic treatments (refrigeration [RF] at −20 and −196 °C using liquid nitrogen) with a target to improve microstructural, thermal, mechanical, and electrochemical responses. The material exhibits densification and grain refinement after these treatments, which improves the physical, thermal, compressive, and corrosion responses. While both RF and liquid nitrogen exposures improve the overall combination of properties, overall improvement in properties is best met with RF treatment at −20 °C. In the results of this work, the efficacy of low energy option (RF) is convincingly established rather than liquid nitrogen exposure (as conventionally practiced) to enhance microstructure and properties.

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Effect of multi‐axial hot forging process on mechanical, and corrosion resistance behavior of Mg‐3Zn alloy for temporary orthopedic implants

Jaiswal

Agrawal

Dubey

et al. 2020

Engineering Reports

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Magnesium (Mg) is a load‐bearing biocompatible material which has the ability to reduce stress shielding effect and facilitate osteocompatibility and biodegradation in the presence of body fluids. However, Mg is highly susceptible to corrosion in the physiological environment, hence leading to poor mechanical integrity. In this study, the multi‐axial hot forging (MAHF) process is performed on Mg‐3Zn alloys to study its grain refinement and possible improvement in mechanical, corrosion, and bioactivity behavior. The average grain size of the sample becomes significantly refined after the third cycle of MAHF. The yield and ultimate compressive strength of Mg‐3Zn alloys are found to increase by 70% and 41%, respectively, after the third cycle of MAHF, which is potentially due to the grain size refinement. Accelerated corrosion studies show improvements in the corrosion resistance with the refined grain structure. Additionally, in‐vitro immersion studies in the simulated body fluid for 14 days showed a reduction in the degradation rate after third cycle of MAHF, due to the increased grain boundary area, which offered more nucleation sites for apatite precipitation. This study underscores and lays the foundation for a new branch of severely deformed fine‐grained Mg‐3Zn alloy for temporary orthopedic implants.

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Bio-inspired low elastic biodegradable Mg-Zn-Mn-Si-HA alloy fabricated by spark plasma sintering

Cited by 76 publications

References 59 publications

Synthesis, Characterization, Corrosion Resistance and In-Vitro Bioactivity Behavior of Biodegradable Mg–Zn–Mn–(Si–HA) Composite for Orthopaedic Applications

Synthesis, Characterization, Corrosion Resistance and In-Vitro Bioactivity Behavior of Biodegradable Mg–Zn–Mn–(Si–HA) Composite for Orthopaedic Applications

Enhancing Microstructural, Thermal, Mechanical, and Corrosion Response of a Bio/Eco‐Compatible Mg–2Zn–1Ca–0.3Mn Alloy Using Two Types of Cryogenic Treatments

Effect of multi‐axial hot forging process on mechanical, and corrosion resistance behavior of Mg‐3Zn alloy for temporary orthopedic implants

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