A nano-fluid was prepared by dispersing 0.1 wt% TiO 2 nano particles in water along with a small amount of surfactant. The performance of the nano-fluid vis-a-vis water as coolant was studied on hot steel plates by measuring the cooling curves and by appropriate metallographic investigations. Significant enhancement in cooling rate was observed for the nano-fluid which could be due to an enhancement of convective heat transfer by jet impingement, coupled with lower surface tension of the nano-fluid, as compared to water.KEY WORDS: TiO 2 nano-fluid; continuous cooling transformation diagram; micro-alloyed steel. 0.14, Al: 0.04, Si: 0.01, S: 0.005, P: 0.013, Ti: 0.029, Nb: 0.004, N: 0.0035 was placed on the sample loading base of the specially constructed experimental set-up as shown in Fig. 2. The nano-fluid was pumped from the tank through a nozzle having a diameter of 6 cm and allowed to fall at a velocity 12.6 m/s on the preheated steel plate. A centrifugal pump with a flow rate of 400 L/h and head of 10 m operated at 230 V (drive: 0.025 kW) was used. A total of nine thermocouples were placed on the surface of the plate where the nano-fluid was incident. The cooling curve of the nanofluid was obtained by plotting the average temperature from the data recorded by all the nine thermocouples versus time. The experiment was repeated by allowing a jet of water on to an equivalent steel plate under the same experimental conditions, and cooling curve of water was plotted in the same manner. A field emission gun scanning electron microscope (FEG SEM), ZEISS, SUPRA 25, Germany operated at 20 kV with EDS attachment was used to study the microstructures taken from the top impinged surfaces as well as from the cross-sections of the plates, cooled by both water and the nano-fluid. An energy dispersive spectroscopic (EDS) analysis was also carried out on the top surface of the plate on which the nano-fluid was incident.
Results and DiscussionFrom Fig. 1 it can be seen that the average size of the asreceived nano particles was in the range of 30 to 50 nm. Figure 3(a) compares the temperature-time plots of the steel plate cooled by water and by water based TiO 2 nanofluid. In the same diagram the temperature time transformation diagram (TTT) and continuous cooling transformation (CCT) plots for the steel composition 4) have been superimposed. The TTT and CCT curves denote 50 % phase transformation.From Fig. 3(a) it is clearly visible that the cooling rate for the water based TiO 2 nano-fluid is much faster than that of water till the bainite start temperature is reached. This difference in the cooling rates produces very distinct changes in the microstructures of the steel plate after cooling by water and by the nano-fluid as shown in Figs. 4(a)-4(e).To begin with, the hot plate right at the onset of cooling will be in the austenite range and phase transformation will occur as cooling progresses. Clearly, polygonal ferrite grains are observed on the top surface of the steel plate where water was incident. By contrast, the sur...