Branch Migration Activity of Rad54 Protein

Mazina, Olga M.; Mazin, Alexander V.

doi:10.1007/978-1-0716-0644-5_11

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2024

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“…Substitution with thiomethoxide followed by Suzuki coupling occurred smoothly to give compound 31 . Importantly, substrate 31 presents an opportunity for diversification at the C5 vector by oxidizing the thioether to the corresponding sulfone, a well-established S N Ar leaving group . Product 32 resulted from the coupling of an alkylzinc halide followed by subsequent addition of an aryl boronic acid.…”

Section: Resultsmentioning

confidence: 99%

Rapid Synthesis of Highly Substituted 1,6-Naphthyridines Via Heteroaryl Ditriflates

Shimkin,

Compton,

Diccianni

et al. 2024

J. Org. Chem.

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We report the discovery of a convenient and efficient method for the synthesis of highly substituted 1,6naphthyridines. A tandem nitrile hydration/cyclization procedure was developed to access 1,6-naphthyridine-5,7-diones under mild conditions. Subsequently, we have found that ditriflation of these intermediates provides 1,6-naphthyridine-5,7-ditriflates which are bench-stable but highly reactive intermediates that can be engaged in one-pot difunctionalization reactions leading to diverse druglike products in rapid fashion.

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Section: Resultsmentioning

confidence: 99%