This paper describes the application of 1H HR-MAS NMR (high-resolution magic angle spinning
nuclear magnetic resonance) to the analysis of durum wheat flours coming from geographical areas
of southern Italy. It is possible to obtain one-dimensional spectra with >80 resonances. With this
technique it is possible to avoid the pretreatment of the samples commonly used in other analytical
techniques. Using one- and two-dimensional NMR methods, some preliminary spectral assignment
were carried out. Finally, it has also been possible to apply a multivariate statistical analysis to
spectral data in a trial of discriminating between the samples.
Keywords: NMR; durum wheat flours; analysis