Characterization of Particle Shape with an Improved 3D Light Scattering Sensor (3D-LSS) for Aerosols

Abstract

To characterize fine particulate products in industrial gas–solid processes, insights into the particle properties are accessible via various measurement techniques. For micron particles, online imaging techniques offer a fast and reliable assessment of their size and shape. However, for the shape analysis of submicron particles, only offline techniques, such as SEM and TEM imaging, are available. In this work, an online sensor system based on the principle of elastic light scattering of particles in the gas phase is developed to measure the shape factor of non-spherical particles in the size range of 500 nm to 5 µm. Single aerosol particles are guided through a monochromatic circularly polarized laser light beam by an aerodynamic focusing nozzle, which was developed based on the CFD simulation of the flow and particle movement. The intensity of the scattered light is measured at several discrete positions in the azimuthal direction around the particles. An algorithm computes the sphericity of the particles based on the distribution of the intensity signals. The sensor construction, data processing and analysis are described. Model aerosols with particles of different shapes are investigated to test the developed sensor and show its performance in the determination of the sphericity distribution of particles.