Chemischer Informationsdienst. Organische Chemie
 1971
DOI: 10.1002/chin.197131336
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ChemInform Abstract: BLDG. VON STABILEN GEMINALEN DIOLEN AUS PYRIDYL‐ UND N,N‐DIMETHYLAMINO‐PHENYL‐TRIFLUORMETHYL‐KETONEN

R. L. Salvador1,
M. Saucier2

Abstract: Die aus entsprechenden Brompyridinen mit tert.‐Butyl‐Li erhaltenen Li‐Pyridine (I) setzen sich mit dem Trifluoracetamid (II) in Äther bei ‐70°C zu den Ketonen (III) um, die bei Luftfeuchtigkeit in die stabilen gem.‐Diole (IV) (57 bis 69,4% Ausbeute) übergehen.

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