ChemInform Abstract: Growth and Characterization of Electrodeposited Na_0.45VOPO₄·1.58H₂O Materials.

Abstract

Growth and Characterization of Electrodeposited Na 0.45 VOPO 4 ·1.58H 2 O Materials. -The title compound is prepared by electrochemical oxidation of VOSO4 in 1M H3PO4 solution to produce a deposit onto a Pt electrode (25 or 60°C, pH 1.9-2.0 adjusted with NaOH, 1.5 or 1.7 V vs. SCE). The samples are characterized by XRD, SEM, and IR spectroscopy. The obtained films comprise fine particles and are of high purity. -(BOUOUD, S.; EL HOURCH, A.; EL KACEMI, K.; GUESSOUS, A.; PRADEL*, A.; RIBES, M.; Solid State Sci. 13 (2011) 12, 2090-2095, http://dx.