Chemischer Informationsdienst. Organische Chemie
 1970
DOI: 10.1002/chin.197016416
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ChemInform Abstract: SYNTH. DES BUFALINS

George R. Pettit1,
L. E. Houghton2,
John Knight3
et al.

Abstract: Zur Synthese des 3β‐Acetoxy‐14‐dehydrobufalins (X) wird Digitoxigenin (I) acetyliert, das 3‐Acetat (II) zur Δ14‐Verbindung (III) dehydratisiert, diese mit Natriummethylat/Methanol in das Lactol und das Lactol durch Erhitzen mit p‐Toluolsulfonsäure/Methanol in das Acetal (IV) (88% Ausbeute, Epimeren‐Gemisch) umgewandelt.

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