ChemInform Abstract: Synthesis and Structure‐Activity Relationships of Potent New Angiotensin Converting Enzyme Inhibitors Containing Saturated Bicyclic Amino Acids.

Blankley, C. John; Kaltenbronn, J. S.; Dejohn, Dana; Werner, A.; Bennett, Leslie R.; Bobowski, George; Krolls, U.; Johnson, D. R.; Pearlman, W. M.; Hoefle, M. L.; Essenburg, Arnold D.; Cohen, Daniel M.; Kaplan, Harvey

doi:10.1002/chin.198747322

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2013

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“…20 The slight difference is visible from superposition of the two structures ( Figure 2). The crystal packing of (1) shows two weak intermolecular C-H…..O contacts (Table 3) …”

Section: Resultsmentioning

confidence: 97%

Crystal Structure of a Perindopril Cyclization Product, C19h30n2o4

Bojarska

Maniukiewicz

Główka

et al. 2013

J. Chil. Chem. Soc.

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The title compound is a product of perindopril intramolecular cyclization. It crystallizes in the tetragonal, non-centrosymmetric space group P4 1 2 1 2 (No. 92) with a = 9.3574(2), b = 9.3574(2), c = 45.6369(9) Å, V = 3996.01(14) Å 3 and Z = 8. The crystal consists of one molecule in the asymmetric unit. The packing exhibits weak intermolecular C-H···O=C contacts forming two C(5) and C(10) chains, which together result in graph-set descriptor R 3 3 (18) motif, running along the crystallographic a-axis.

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“…20 The slight difference is visible from superposition of the two structures ( Figure 2). The crystal packing of (1) shows two weak intermolecular C-H…..O contacts (Table 3) …”

Section: Resultsmentioning

confidence: 97%