2013
DOI: 10.1002/chin.201327017
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ChemInform Abstract: Synthesis, Crystal Structure, and Variable‐Temperature‐Luminescent Property of the Organically Templated Pentaborate [C10N2H9] [B5O6(OH)4] ·H3BO3·H2O.

Abstract: Synthesis, Crystal Structure, and Variable-Temperature-Luminescent Property of the Organically Templated Pentaborate [C10N2H9][B5O6(OH)4]·H3BO3·H2O. -Colorless block crystals of the title compound are prepared by addition of boric acid to a solution of 4,4'-bipyridine in water (90°C, 68% yield). The compound crystallizes in the triclinic space group P1 with Z = 2 (single crystal XRD). The structure contains monoprotonated bipyridinium cations, [B 5 O 6 (OH) 4 ]anions, and H 3 BO 3 and H 2 O molecules. The bicy… Show more

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