Surface areas of cottons differing in variety and maturity, and cottons that had been subj ected t o various physical and chemical t reat m ents wer e meas ured before and after swelling. Swollen cottons were prepared by immersing air-dried cot tons in wat er a t roo m t emperature for 24 houl's, displacing the water wi th m etha nol and t h e m ethanol wi th p entane, and fin a lly drying the fibers. Surface areas were calculated from the quantity of nitrogen ad sorbed a t -195.8° C.The specific surfaces of unswollen fib ers were less t han 1 square m eter p er gram ; t hose of the swollen fib ers ranged fr om 4 to 148 quare m eters p er gram . Purificat ion and m erceri zation produ ced in creases in th e surface ava ilable a fte r s welling; m eth ylenat ion produced a d ecrease; eth ylamine t rea t ment had no effect. In t he early stages of m ethanolysis, a d ecrease in t he surface availa ble after swelling occUl'red ; in th e later stages, a n incr ease.Although urface area m easuremen ts were p ro bably i n no instance made on completely swollcn fiber, the procedure employed is believed to be useful in evaluat ing th e effects of vari ous t reatments 011 cotto n and other cellulose fibers.