Comprehensive assessment of clean-up strategies for optimizing an analytical multi-method to determine pesticides and mycotoxins in Brazilian medicinal herbs using QuEChERS-LC-TQ-MS/MS

Zorzella Fontana, Marlos Eduardo; Caiel da Silva, Rosselei; Duarte dos Santos, Ingrid; Neu, Júlia Paula; Wouters, Robson Dias; Babinski, Paola Jennifer; Hoffmann, Jessica Fernanda; Rossi, Rochele Cassanta; Essi, Liliana; Pizzutti, Ionara Regina

doi:10.1039/d4ay00599f

Anal. Methods

2024

DOI: 10.1039/d4ay00599f

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Comprehensive assessment of clean-up strategies for optimizing an analytical multi-method to determine pesticides and mycotoxins in Brazilian medicinal herbs using QuEChERS-LC-TQ-MS/MS

Marlos Eduardo Zorzella Fontana,

Rosselei Caiel da Silva,

Ingrid Duarte dos Santos

et al.

Abstract: The use of medicinal herbs has increased significantly, however the presence of pesticide residues and mycotoxins has generated constant discussion and concern among regulatory agencies. Developing and validating an analytical...

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Recent Review of the Quechers Sample Preparation Method for Food and Environmental Sample Analysis

Shinkafi,

Lawal,

Gwaram

et al. 2024

FJS

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Creating reliable, environmentally responsible, and effective processes that ensure the traceability, safety, and caliber of their results is one of the main challenges facing researchers doing multi-residue analysis. The QuEChERS which stands for Quick, Easy, Cheap, Effective, Rugged, and Safe method has shown itself to be highly adaptable, yielding positive outcomes with a range of analytes. This method allows for versatility in the choice of solvents, salts, and buffers for salting-out partitioning, as well as the use of various sorbents throughout the cleanup process. QuEChERS is a more environmentally friendly sample preparation technique that fits perfectly with analytical chemistry's rising emphasis on sustainability. This review paper's goal is to illustrate the primary applications of the QuEChERS sample preparation method, with a focus on food and environmental investigations. It also covers important improvements in the history of sample preparation methods and offers insights into the classes of substances that have been effectively evaluated with this methodology.

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Recent Review of the Quechers Sample Preparation Method for Food and Environmental Sample Analysis

Shinkafi,

Lawal,

Gwaram

et al. 2024

FJS

View full text Add to dashboard Cite

show abstract

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Comprehensive assessment of clean-up strategies for optimizing an analytical multi-method to determine pesticides and mycotoxins in Brazilian medicinal herbs using QuEChERS-LC-TQ-MS/MS

Abstract: The use of medicinal herbs has increased significantly, however the presence of pesticide residues and mycotoxins has generated constant discussion and concern among regulatory agencies. Developing and validating an analytical...

Cited by 1 publication

References 52 publications

Recent Review of the Quechers Sample Preparation Method for Food and Environmental Sample Analysis

Recent Review of the Quechers Sample Preparation Method for Food and Environmental Sample Analysis

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