2020
DOI: 10.3390/ma13163529
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Consequences of Different Mechanical Surface Preparation of Ni-Base Alloys during High Temperature Oxidation

Abstract: The influence of surface roughness on its high temperature oxidation for an Ni-base superalloy was studied using laser profilometry, atomic force microscopy, mass change measurements, glow-discharge optical emission spectrometry, scanning electron microscopy, X-ray diffraction, and positron annihilation methods. The isothermal and cyclic air oxidation tests were performed at 1000 °C and showed dependence of oxidation behavior on surface roughness. Smoother surfaces oxidation resulted in the formation of a mult… Show more

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Cited by 9 publications
(6 citation statements)
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“…Previous studies have shown that annihilation techniques can be successfully used to analyze the surface layer of shot- peened unalloyed steel, titanium, and aluminum alloys [ 25 ], and stainless steel [ 26 ]. Additionally, nickel superalloys similar to that analyzed in this study have been investigated with these techniques [ 27 , 28 , 29 , 30 , 31 , 32 ], and interesting results were reported. Contrary to the other methods mentioned above, positron annihilation provides information about the structure of sample defects (both their size and concentration) at the atomic level.…”
Section: Introductionmentioning
confidence: 99%
“…Previous studies have shown that annihilation techniques can be successfully used to analyze the surface layer of shot- peened unalloyed steel, titanium, and aluminum alloys [ 25 ], and stainless steel [ 26 ]. Additionally, nickel superalloys similar to that analyzed in this study have been investigated with these techniques [ 27 , 28 , 29 , 30 , 31 , 32 ], and interesting results were reported. Contrary to the other methods mentioned above, positron annihilation provides information about the structure of sample defects (both their size and concentration) at the atomic level.…”
Section: Introductionmentioning
confidence: 99%
“…Another proposed explanation of different oxidation behavior of studied material is that more rough surface preparation introduces higher amount of defects which can act as an easy diffusion path for the elements forming protective oxide scale (Cr, Mn and Si in the present case) as it was already proposed in previous works (Ref [21][22][23][24]34). For quantitative description of the influence of surface geometry in term of surface roughness, time-to-failure was calculated for each specimen tested in all kind of cyclic oxidation test.…”
Section: Discussionmentioning
confidence: 68%
“…Therefore, from an electro-technical point of view, an oxide film's capacitance and resistance are connected in parallel. The capacitive properties of the film appear at times t 0 ≤ εε 0 ρ ≈ 3 (10 −8 -10 −6 ) sec [18]. The maximum electric field strength due to the accumulation of charge on the oxide film over this time is defined as…”
Section: Methodsmentioning
confidence: 99%