Corrigendum to “Controlled mechano-chemical synthesis of nanostructured ternary complex hydride Mg2FeH6 under low-energy impact mode with and without pre-milling”[J. Alloys Comp. 384 (2004) 231–248]

Li, Songlin; Varin, R.A.; Morozova, O. S.; Khomenko, T. I.

doi:10.1016/s0925-8388(04)01363-5

Cited by 12 publications

(40 citation statements)

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“…2b by deep endothermic peaks, within the temperature range of ∼321-329 • C. The H 2 amount from TGA test was estimated at ∼2.5 wt.%. Additional TPD test [14] confirmed the desorption of ∼3.8 wt.% hydrogen at ∼306 • C (Fig. 2c).…”

Section: Resultsmentioning

confidence: 62%

“…Similarly to the behavior of MgH 2 , the DSC hydrogen desorption peak temperature of the nanostructured ternary complex hydride Mg 2 FeH 6 and the duplex mixture (␤-MgH 2 + Mg 2 FeH 6 ), synthesized in a number of differently milled Mg-Fe and 2Mg-Fe mixtures [14,15], does not seem to depend on the initial nanograin (crystallite) size of Mg 2 FeH 6 (within the investigated range 2-8 nm) (Fig. 6b).…”

Section: Resultsmentioning

confidence: 99%

“…More extensive details of milling procedures can be found in a number of Refs. [11][12][13][14][15]. Morphological and microstructural examination of powders was conducted using high-resolution, field emission SEM (FE SEM) LEO 1530 equipped with integrated EDAX Pegasus 1200 EDS/OIM and X-ray diffraction [11][12][13][14][15].…”

Section: Methodsmentioning

confidence: 99%

“…[11][12][13][14][15]. Morphological and microstructural examination of powders was conducted using high-resolution, field emission SEM (FE SEM) LEO 1530 equipped with integrated EDAX Pegasus 1200 EDS/OIM and X-ray diffraction [11][12][13][14][15]. Thermal behavior was investigated by DSC, TGA [13][14][15] and temperature programmed desorption (TPD) [14,15].…”

Section: Methodsmentioning

confidence: 99%

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Nanocrystalline and non-crystalline hydrides synthesized by controlled reactive mechanical alloying/milling of Mg and Mg–X (X = Fe, Co, Mn, B) systems

Varin

Chiu

et al. 2005

Journal of Alloys and Compounds

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Section: Resultsmentioning

confidence: 62%

Section: Resultsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%

Section: Methodsmentioning

confidence: 99%

See 2 more Smart Citations

Nanocrystalline and non-crystalline hydrides synthesized by controlled reactive mechanical alloying/milling of Mg and Mg–X (X = Fe, Co, Mn, B) systems

Varin

Chiu

et al. 2005

Journal of Alloys and Compounds

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“…For the preparation of Mg 2 FeH 6 compounds, many methods such as sintering the 2Mg+Fe mixture under high pressure hydrogen 5,6) and mechanical milling the 2Mg+Fe or 2MgH 2 +Fe mixture [7][8][9][10][11][12][13][14] have been developed. The Mg 2 FeH 6 compound has been first synthesized and described in 1984.…”

Section: Introductionmentioning

confidence: 99%

Synthesis and Hydrogen Storage Behaviour of Pure Mg<SUB>2</SUB>FeH<SUB>6</SUB> at Nanoscale

et al. 2011

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Pure Mg 2 FeH 6 compounds with two different morphologies have been successfully synthesized directly by mechanical milling (MM) and sintering of a mixture of 2Mg+Fe nanoparticles under an H 2 atmosphere, respectively. The successful preparation of pure Mg 2 FeH 6 can be attributed to the small particle sizes of Mg and Fe nanoparticles prepared by hydrogen plasma-metal reaction (HPMR), which provides shorter diffusion distance for hydrogen and the metals. The X-ray diffraction (XRD) and scanning electron microscopy (SEM) results show that the Mg 2 FeH 6 synthesized by mechanical milling has larger particle size but smaller crystallite size compared with the Mg 2 FeH 6 synthesized by sintering. The Mg 2 FeH 6 synthesized by mechanical milling can desorb more than 4.5 mass% hydrogen in 10 min under an initial hydrogen pressure of 0.001 bar at 573 K. Compared with the Mg 2 FeH 6 synthesized by sintering under the same conditions as the Mg 2 FeH 6 synthesized by mechanical milling, it is suggested that decrease of crystallite size is beneficial for enhancing desorption property of Mg 2 FeH 6 .

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The effect of sequential and continuous high-energy impact mode on the mechano-chemical synthesis of nanostructured complex hydride Mg2FeH6

Varin

Wronski

et al. 2005

Journal of Alloys and Compounds

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Corrigendum to “Controlled mechano-chemical synthesis of nanostructured ternary complex hydride Mg2FeH6 under low-energy impact mode with and without pre-milling”[J. Alloys Comp. 384 (2004) 231–248]

Cited by 12 publications

References 0 publications

Nanocrystalline and non-crystalline hydrides synthesized by controlled reactive mechanical alloying/milling of Mg and Mg–X (X = Fe, Co, Mn, B) systems

Nanocrystalline and non-crystalline hydrides synthesized by controlled reactive mechanical alloying/milling of Mg and Mg–X (X = Fe, Co, Mn, B) systems

Synthesis and Hydrogen Storage Behaviour of Pure Mg<SUB>2</SUB>FeH<SUB>6</SUB> at Nanoscale

The effect of sequential and continuous high-energy impact mode on the mechano-chemical synthesis of nanostructured complex hydride Mg2FeH6

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