Deep Eutectic Solvents, Bio-Based Solvents, and Surfactant for Green Sample Pretreatment and Determination

Lakshmipraba, J.; Prabhu, Rupesh N.

doi:10.1007/978-3-030-96534-1_9

Green Chemical Analysis and Sample Preparations 2022

DOI: 10.1007/978-3-030-96534-1_9

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Deep Eutectic Solvents, Bio-Based Solvents, and Surfactant for Green Sample Pretreatment and Determination

J. Lakshmipraba,

Rupesh N. Prabhu

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2024

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Cited by 1 publication

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Selective and fast oxidation of alcohol to aldehyde using novel catalytic deep eutectic solvent surfactants

Shokr Chalaki,

Azizi,

Mirjafary

et al. 2024

Front. Chem.

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Deep eutectic solvent (DES) has been considered as a useful catalyst and reaction medium for various organic transformations. Herein, we report the catalytic application of novel deep eutectic solvent- based surfactant (DES surfactant) for the selective and fast oxidation of alcohols to aldehydes. The readily accessible DES surfactants (FeCl3/BHDC) was prepared using inexpensive ferric chloride (FeCl3) and benzyl hexadecyl dimethyl ammonium chloride in a simple manner. The synthesized FeCl3/BHDC was characterized using various techniques, including, FTIR spectroscopy, thermal gravimetric analysis (TGA), scanning electron microscopy (SEM), and energy- dispersive X-ray spectroscopy (EDS) to determine its structure. The catalytic activity of FeCl3/BHDC in the selective oxidation of various alcohols to corresponding aldehyde derivative was investigated. The results showed the reaction could be completed within very short reaction times ranging from 2 to 15 min, while achieving good to excellent yields. This protocol offers a facile strategy and excellent efficiency in selectively oxidizing various alcohol derivatives to their respective aldehydes and ketones, utilizing hydrogen peroxide in the presence of catalytic DES surfactant.

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Selective and fast oxidation of alcohol to aldehyde using novel catalytic deep eutectic solvent surfactants

Shokr Chalaki,

Azizi,

Mirjafary

et al. 2024

Front. Chem.

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show abstract

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Deep Eutectic Solvents, Bio-Based Solvents, and Surfactant for Green Sample Pretreatment and Determination

Cited by 1 publication

References 143 publications

Selective and fast oxidation of alcohol to aldehyde using novel catalytic deep eutectic solvent surfactants

Selective and fast oxidation of alcohol to aldehyde using novel catalytic deep eutectic solvent surfactants

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