Development of a fluorescent probe for cefazolin detection based on solvent-based de-emulsification dispersive liquid–liquid microextraction of silver nanoparticles

FeS2 nanosheets–luminol–O2 chemiluminescence method for determination of venlafaxine hydrochloride, imipramine hydrochloride, and cefazolin sodium

“…Furthermore, it outperforms spectrophotometry [24] and CL employing KMnO 4 ‐H 2 SO 4 reaction [34] in the analysis of IPM, as well as differential pulse voltammetry [31] and CL utilizing CuO NPs–luminol–H 2 O 2 reaction [35] in the analysis of CEF. Moreover, based on the data presented in Table S2, the analytical methods that demonstrated superior performance compared to the CL method developed in this study involved HPLC [19, 20], spectrofluorimetry [26], and CL utilizing tris (2,2′‐bipyridyl)ruthenium (II)–peroxydisulfate reaction [32] for VEX analysis, CL involving N ‐bromosuccinimide‐H 2 O 2 [33] for IPM analysis, and HPLC [22] and spectrofluorimetry [28] for CEF analysis. Other techniques presented in Table S2 exhibited almost comparable analytical parameters to those of the CL method developed in this study.…”

“…Certain fluorescence methods mentioned in Table S2 pose challenges in their implementation. For example, certain experiments require heating the solution [27] or performing them in an organic solvent [28].…”

“…The CL system developed in this study shows promising potential for the analysis of several pharmaceuticals, including VFX, IPM, and CEF, and its linear ranges enable convenient monitoring of the concentrations of these pharmaceuticals in pharmaceutical products. Furthermore, compared to HPLC [19, 20, 22] and spectrofluorimetry [26, 28], the method developed in this study has advantages such as simplicity and cost effectiveness in terms of the necessary equipment.…”

“…(2,2 0 -bipyridyl)ruthenium (II)-peroxydisulfate reaction [32] for VEX analysis, CL involving N-bromosuccinimide-H 2 O 2 [33] for IPM analysis, and HPLC [22] and spectrofluorimetry [28] for CEF analysis. Other techniques presented in Table S2 exhibited almost comparable analytical parameters to those of the CL method developed in this study.…”

“…Various methodologies, such as high-performance liquid chromatography (HPLC) [19][20][21][22], spectrophotometry [23][24][25], spectroflourimetry [26][27][28], electrochemical [29][30][31], and CL [32][33][34][35][36] methods, have been developed for the quantification of VFX, IPM, and CEF.…”