Development of Microwave-Assisted Hydrothermal Extraction Coupled to Ion Chromatography for Comprehensive Analysis of Chemical Composition in Intracorporeal Stone

A green and simple method, dynamic microwave-assisted micelle extraction coupled with cloud point preconcentration, was developed for the determination of triazine herbicides in soil samples. The method has the advantages of those two extraction procedures, which could eliminate the interferences from complex soil samples greatly. Non-ionic surfactant Triton X-114 aqueous solution used as extraction solvent was continuously pumped into soil samples. The resulting extract was heated and centrifuged in the presence of NaCl. After centrifugation, the analytes were enriched into the surfactant-rich phase. No filtration or cleaning steps were required. Several key parameters were investigated. The Box–Behnken design was applied to optimize the experimental factors involved in the dynamic microwave-assisted micelle extraction. Good linearity was observed in the range of 1.00–250.00 μg kg−1. The limits of detection were ranged between 0.26 and 1.71 μg kg−1. The recoveries of analytes ranged from 80.3 to 98.3% with the relative standard deviations ranging from 1.1 to 6.6%.

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Development of Microwave-Assisted Hydrothermal Extraction Coupled to Ion Chromatography for Comprehensive Analysis of Chemical Composition in Intracorporeal Stone

Cited by 2 publications

References 24 publications

Field sample preparation of trace inorganic anions in environmental waters with in-tip microextraction device based on anion-exchange monolithic adsorbent followed by ion chromatography quantification

Field sample preparation of trace inorganic anions in environmental waters with in-tip microextraction device based on anion-exchange monolithic adsorbent followed by ion chromatography quantification

Dynamic Microwave-Assisted Micelle Extraction Coupled with Cloud Point Preconcentration for the Determination of Triazine Herbicides in Soil

Contact Info

Product

Resources

About