This paper examines the effect of microstructure and mechanical properties of aluminium alloy. Aluminium and its alloys have been indentified as an important and useful engineering material. It is attracted by its various unique properties, such as appearance, strength-to-weight ratio, excellent thermal properties, workability properties and good mechanical behaviour. In this experiment, there were 2 sets (7 samples each) aluminium alloy prepared. Prepared specimens quenched for one hour by two different media (water & cow urine). Specimens prepared to apply tensile, yield strength and hardness test and show the effect of medias cooling rate on mechanical properties and microstructure of all specimens examined. In water media tensile, yield strength and hardness were improved, cow urine contributed in decrease tensile and yield strength properties because grain size larger, but hardness slightly improved.