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Mud shale is characterized by low strength and strong swelling, with rheological effects and deformation caused by drilling fluid and formation water. Establishing a rheological model to characterize the deformation characteristics is key to solving the problem of wellbore stability. The influence of moisture content on rock strength and creep mechanical properties were studied by means of water absorption, uniaxial compression, and creep tests. The tests showed that with the increase in moisture content, the elastic modulus and strength of hard brittle mud shale decreased. Further, under the same load, the instantaneous strain increased with increasing moisture content. Meanwhile, under various loading stresses, rock creep exhibited non-linear characteristics, which can be divided into three different creep stages: attenuated creep, stable creep, and accelerated creep. Starting with a non-linear viscous dashpot, and then introducing aging degradation and water-bearing weakening effects, based on the water-bearing creep characteristics of hard brittle shale as well as the modeling ideas of the classic component combination model, a new improved creep model based on the Nishihara model was established to describe the characteristics of the accelerated creep stage of hard brittle mud shale with various moisture contents. Subsequently, the Levenberg–Marquardt non-linear, least-squares method was adopted to invert the creep parameters. The results showed that the simulated creep curves achieved by employing the new creep model were consistent with the experimental results, thereby confirming the ability of the new non-linear creep model to provide a theoretical reference for the study of wellbore stability of hard brittle mud shale.
Mud shale is characterized by low strength and strong swelling, with rheological effects and deformation caused by drilling fluid and formation water. Establishing a rheological model to characterize the deformation characteristics is key to solving the problem of wellbore stability. The influence of moisture content on rock strength and creep mechanical properties were studied by means of water absorption, uniaxial compression, and creep tests. The tests showed that with the increase in moisture content, the elastic modulus and strength of hard brittle mud shale decreased. Further, under the same load, the instantaneous strain increased with increasing moisture content. Meanwhile, under various loading stresses, rock creep exhibited non-linear characteristics, which can be divided into three different creep stages: attenuated creep, stable creep, and accelerated creep. Starting with a non-linear viscous dashpot, and then introducing aging degradation and water-bearing weakening effects, based on the water-bearing creep characteristics of hard brittle shale as well as the modeling ideas of the classic component combination model, a new improved creep model based on the Nishihara model was established to describe the characteristics of the accelerated creep stage of hard brittle mud shale with various moisture contents. Subsequently, the Levenberg–Marquardt non-linear, least-squares method was adopted to invert the creep parameters. The results showed that the simulated creep curves achieved by employing the new creep model were consistent with the experimental results, thereby confirming the ability of the new non-linear creep model to provide a theoretical reference for the study of wellbore stability of hard brittle mud shale.
Summary The sustained conductivity of hydraulic/acid fractures is crucial for the continuous and effective production of hydrocarbons. However, hydraulic fractures in soft carbonate formations often experience a reduction in conductivity due to rock deformation and creeping under in-situ stresses. One approach to resolve this issue is to stiffen the fracture surfaces using a consolidating agent. This study examines the application of diammonium hydrogen phosphate (DAP) as an additive to improve the hydraulic/acid fracture conductivity in Indiana limestone and Austin chalk slabs. Initially, flat slabs of Indiana limestone and Austin chalk were subjected to acidization using 15% and 10% hydrochloric acid (HCl) for 10 minutes and 5 minutes, respectively. The resulting surface texture changes were measured using a profilometer. Subsequently, half of the samples underwent treatment in 1 M DAP under 1,000 psi and 75°C for 72 hours. The surface stiffness of the samples was evaluated using nondestructive impulse hammering before and after acid injection and DAP treatment, while hydraulic/acid fracture conductivity was determined using an API conductivity setup. Following acid injection, the experimental results demonstrate that the stiffness of all the samples was diminished to different degrees. However, intact Indiana limestone samples exhibited increased stiffness after treatment with DAP. Acidized Indiana limestone samples showed partial restoration of their original stiffness with DAP treatment. In contrast, DAP treatment fully restored the stiffness of Austin chalk samples and further enhanced it, resulting in a twofold to fivefold increase. The increased stiffness observed in the treated samples had a direct impact on short- and long-term conductivity. Treated Indiana limestone fractures exhibited double the conductivity of untreated fractures. The improvement in Austin chalk conductivity was even more significant after DAP treatment, resulting in seven to eight times higher conductivity in the treated hydraulic/acid fractures. It is worth noting that there was little to no correlation between surface roughness and conductivity, highlighting the significant influence of fracture stiffness on conductivity.
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