Extraction of Eugenol from Essential Oils by In Situ Formation of Deep Eutectic Solvents: A Green Recyclable Process

Shen, Lingqi; Jin, Xiangzi; Zhang, Zhihui; Yi, Yuexing; Zhang, Jingyu; Li, Zuguang

doi:10.1007/s41664-023-00267-x

J. Anal. Test.

2023

DOI: 10.1007/s41664-023-00267-x

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Extraction of Eugenol from Essential Oils by In Situ Formation of Deep Eutectic Solvents: A Green Recyclable Process

Lingqi Shen,

Xiangzi Jin,

Zhihui Zhang

et al.

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Cited by 4 publications

References 38 publications

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Antimicrobial and acaricide sanitizer tablets produced by wet granulation of spray-dried soap and clove oil-loaded microemulsion

Gross,

Lima,

Sousa

et al. 2024

PLoS ONE

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A novel sanitizer tablet containing clove essential oil (CO) microemulsion was developed. A preformulation study using nuclear magnetic resonance and thermal analyses showed component compatibility. The main components of the samples remained intact despite a color change, probably due to a strong acid-base interaction between eugenol and diethanolamine. The CO microemulsion showed acaricidal and larvicidal activities superior to the commercial product, with product efficacy of 99.9% and larvae mortality of 94%. Optimal spray-drying conditions were achieved with inlet and outlet temperatures of 50°C and 40°C, respectively, an aspiration rate of 1 m3 min⁻1, and a 0.25 L h⁻1 injection flow. The feed suspension comprised 50% (v/v) liquid soap, 37.5% (v/v) water, 12.5% (v/v) ethanol, and 5.0% (w/v) silica. This formulation and processing parameters allowed for successful free-flow powder formation, providing a suitable matrix for incorporating the CO microemulsion via wet granulation without heating. Finally, sanitizer tablets produced from such granules resulted in a uniform product with low weight variation (coefficient of variation of 0.15%), eugenol content of 95.5% ± 3.3, and friability of 0.58%. Furthermore, the tablets showed rapid aqueous dispersion, forming a colloidal system with particle sizes of 221 nm and a zeta potential of -17.2 mV. Antimicrobial activity tests demonstrated the effectiveness of the sanitizer tablet against bacteria and fungi, exhibiting comparable antimicrobial potency to isolated CO. Hence, the sanitizer tablet developed represents a promising candidate as a practical and efficient solution for pest control, offering strong antimicrobial and acaricidal activity.

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Extraction of Eugenol from Essential Oils by In Situ Formation of Deep Eutectic Solvents: A Green Recyclable Process

Cited by 4 publications

References 38 publications

In Situ Analysis of Tobacco Leaves Based on Microwave Plasma Torch Desorption Ionization Mass Spectrometry

In Situ Analysis of Tobacco Leaves Based on Microwave Plasma Torch Desorption Ionization Mass Spectrometry

A signal amplifying photoelectrochemical immunosensor based on the synergism of Au@CoFe2O4 and CdS/NiCo2O4 for the sensitive detection of neuron-specific enolases

Antimicrobial and acaricide sanitizer tablets produced by wet granulation of spray-dried soap and clove oil-loaded microemulsion

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