Facile Synthesis, Crystal Structure, Spectral Characterization, Quantum Chemical Calculations, and Hirshfeld Surface Analysis of 5‐Chloro‐3‐Methoxy‐4‐Hydroxybenzaldehyde
Abstract:This article deals with synthesis, growth, structure, and characterization of 5-chloro-3-methoxy-4-hydroxybenzaldehyde (5CMHBA or 5-chlorovanillin) single crystals. A facile one-pot method is employed for the chlorination of vanillin using N-chlorosuccinimide. After chlorination, the single crystals of 5CMHBA are grown by slow evaporation solution growth technique. Grown crystals are subjected to single crystal X-ray diffraction (SXRD), Fourier Transform Infrared (FTIR), and Thermogravimetric-Differential Ther… Show more
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