High velocity oxy-fuel thermal spraying was used to prepare free-standing CoNiCrAlY ) bond coat alloy samples approximately 0.5 mm thick. Creep tests were conducted at 750 C on these samples using a small punch (SP) creep test method. The samples were characterised before and after creep testing using scanning electron microscopy with electron backscatter diffraction (EBSD). EBSD revealed a two phase fcc -Ni and bcc B2 β-NiAl microstructure with grain sizes ~ 1-2 m for both phases, which did not change significantly following testing. The constant temperature SP test data were characterised by a minimum creep strain rate, , and a total time to failure, t f , at different applied stresses. The data are fitted to conventional power law equations with a stress exponent for creep close to 8 in the Norton power law and between 7 and 10 in the Monkman-Grant creep rupture law. Creep rupture was predominantly due to creep cavitation voids nucleating at both the γ -β interphase boundaries and the - grain boundaries leading to final failure by void linkage. However, rupture life was influenced by the quantity of oxide entrained in the coating during the spray deposition process.