2022
DOI: 10.1002/ange.202207206
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High‐Humidity Shaker Aging to Access Chitin and Cellulose Nanocrystals**

Abstract: To unlock nature's potential for functional biomaterials, many efforts have been devoted to isolating the nanocrystalline domains within the supramolecular structure of polysaccharides. Yet, low reactivity and yield in aqueous systems along with excessive solvent usage hinders its development. In this report, the first solvent‐free pathway to access carboxylated chitin and cellulose nanocrystals with excellent mass balance is described, relying on a new method coined high‐humidity shaker aging (HHSA). The meth… Show more

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