Highly efficient dispersive liquid-liquid microextraction assisted by magnetic porous carbon composite-based dispersive micro solid-phase extraction for determination of tramadol and methadone in urine samples by gas chromatography-mass spectrometry

Isazad, Monireh; Amirzehni, Maliheh; Akhgari, Maryam

doi:10.1016/j.chroma.2022.462989

Cited by 19 publications

(3 citation statements)

References 33 publications

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“…Pyrolysis is a method to change the structure of Fe-MOF by placing Fe-MOF templates in an oxygen-free environment at high temperature. For example, using FeCl 3 ·6H 2 O and 2-NH 2 -TA as raw materials, Isazad et al synthesized the precursor material NH 2 -MIL-88B using the solvothermal method; then, the prepared MOFs were pyrolyzed in an Ar atmosphere to obtain Fe 3 O 4 @C particles [ 73 ].…”

Section: Synthesis Methodsmentioning

confidence: 99%

“…Lsazad et al took NH 2 -MIL-88B as the initial raw material and then pyrolyzed it in an Ar atmosphere to obtain a Fe 3 O 4 @C composite material. Studies have proven that the material can be used in a micro-solid phase extract, two-liquid phase micro-extract, GC-MS detection system for the identification and determination of tramadol and methadone in urine samples, which can be completed at the same time [ 73 ]. Qian et al used Fe-MIL-88B as a template and obtained Fe 3 O 4 /carbon ( Figure 2 f) particles by pyrolysis, which were used to deliver DOX for tumor therapy.…”

Section: Classification Of Fe-based Mofsmentioning

confidence: 99%

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Fe-Based Metal Organic Frameworks (Fe-MOFs) for Bio-Related Applications

Zhu

Cai

et al. 2023

Pharmaceutics

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Metal–organic frameworks (MOFs) are porous materials composed of metal ions and organic ligands. Due to their large surface area, easy modification, and good biocompatibility, MOFs are often used in bio-related fields. Fe-based metal–organic frameworks (Fe-MOFs), as important types of MOF, are favored by biomedical researchers for their advantages, such as low toxicity, good stability, high drug-loading capacity, and flexible structure. Fe-MOFs are diverse and widely used. Many new Fe-MOFs have appeared in recent years, with new modification methods and innovative design ideas, leading to the transformation of Fe-MOFs from single-mode therapy to multi-mode therapy. In this paper, the therapeutic principles, classification, characteristics, preparation methods, surface modification, and applications of Fe-MOFs in recent years are reviewed to understand the development trends and existing problems in Fe-MOFs, with the view to provide new ideas and directions for future research.

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Section: Synthesis Methodsmentioning

confidence: 99%

Section: Classification Of Fe-based Mofsmentioning

confidence: 99%

Fe-Based Metal Organic Frameworks (Fe-MOFs) for Bio-Related Applications

Zhu

Cai

et al. 2023

Pharmaceutics

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“…Colorimetry 19 , chemiluminescence (CL) 20 , HPLC 21 – 23 , spectrophotometry 24 , 25 , and electrophoresis 26 , 27 have been employed to detect SER and TRA. However, these methods lack sensitivity and stability and are time-consuming.…”

Section: Introductionmentioning

confidence: 99%

Quantification of tramadol and serotonin by cobalt nickel tungstate in real biological samples to evaluate the effect of analgesic drugs on neurotransmitters

Zafar,

Wasim,

Fatima

et al. 2023

Sci Rep

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In this work, CoNiWO4 nanocomposite was used as an electrochemical sensor for the simultaneous electrochemical detection of tramadol and serotonin. The nanocomposite was synthesized using a hydrothermal method and characterized via XRD, SEM, TGA, Zeta, UV, and FTIR. The sensor was developed by depositing CoNiWO4-NPs onto the glassy carbon electrode surface. Tramadol and serotonin were detected by employing cyclic voltammetry (CV), differential pulse voltammetry (DPV), electrochemical impedance spectroscopy (EIS), and chronoamperometry. Analytes were detected at different pH, concentrations, and scan rates. The prepared sensor showed a 0–60 µM linear range, with a LOD of 0.71 µM and 4.29 µM and LOQ of 14.3 µM and 2.3 µM for serotonin and tramadol, respectively. Finally, the modified electrode (CoNiWO4–GCE) was applied to determine tramadol and serotonin in biological samples.

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Recent Progress and Applications of Advanced Nanomaterials in Solid‐Phase Extraction

Chen,

Zhang,

Yin

et al. 2024

Electrophoresis

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Sample preparation maintains a key bottleneck in the whole analytical procedure. Solid‐phase sorbents (SPSs) have garnered increasing attention in sample preparation research due to their crucial roles in achieving high clean‐up and enrichment efficiency in the analysis of trace targets present in complex matrices. Novel nanoscale materials with improved characteristics have garnered considerable interest across different scientific disciplines due to the limited capabilities of traditional bulk‐scale materials. The purpose of this review is to offer a thorough summary of the latest developments and uses of SPSs in preparing samples for chromatographic analysis, focusing on the years 2020–2024. The techniques for preparing SPSs are examined, such as metal–organic frameworks (MOFs), covalent organic frameworks (COFs), carbon nanoparticles (CNPs), molecularly imprinted polymers (MIPs), and metallic nanomaterials (MNs). Examining the pros and cons of different extraction methods, including solid‐phase extraction (SPE), magnetic SPE (MSPE), flow‐based SPE (FBA‐SPE), solid‐phase microextraction (SPME), stir‐bar sorptive extraction (SBSE), and dispersive SPE (DSPE), is the main focus. Furthermore, this article presents the utilization of SPE technology for isolating common contaminants in various environmental, biological, and food specimens. We highlight the persistent challenges in SPSs and anticipate future advancements and applications of novel SPSs.

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Highly efficient dispersive liquid-liquid microextraction assisted by magnetic porous carbon composite-based dispersive micro solid-phase extraction for determination of tramadol and methadone in urine samples by gas chromatography-mass spectrometry

Cited by 19 publications

References 33 publications

Fe-Based Metal Organic Frameworks (Fe-MOFs) for Bio-Related Applications

Fe-Based Metal Organic Frameworks (Fe-MOFs) for Bio-Related Applications

Quantification of tramadol and serotonin by cobalt nickel tungstate in real biological samples to evaluate the effect of analgesic drugs on neurotransmitters

Recent Progress and Applications of Advanced Nanomaterials in Solid‐Phase Extraction

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