2003
DOI: 10.1039/b212266a
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Hydrothermal synthesis and crystal structure of two Co phosphonates containing trifunctional phosphonate anions: Co3(O3PCH2NH2CH2PO3)2 and Co3(O3PCH2-NC4H7-CO2)2·5H2O

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Cited by 65 publications
(49 citation statements)
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“…In 2, the nitrogen atoms are protonated by H 2 PO 4 Ϫ groups. These results are supported by the 13 C MAS NMR and IR spectra of 2 (Figures 3 and 4).…”
Section: Resultssupporting
confidence: 87%
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“…In 2, the nitrogen atoms are protonated by H 2 PO 4 Ϫ groups. These results are supported by the 13 C MAS NMR and IR spectra of 2 (Figures 3 and 4).…”
Section: Resultssupporting
confidence: 87%
“…This method, which is based on a literature technique, [13] gave H 3 PMP and H 3 PMTA from the corresponding amino acids in a Mannich-type reaction in yields of 96% and 85%, respectively. γ-ZrP was prepared according to the reported procedure.…”
Section: Resultsmentioning
confidence: 99%
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“…ORTEP representation of the asymmetric unit of compound 1; thermal ellipsoids are drawn at the 50% probability level (7) Co (2)ϪO (22)#3 2.049(6) Co(1)ϪO (12) Co(1)ϪO (23) 2.063 (7) Co (2)ϪO(2W)#3 2.121(7) Co(1)ϪO (13)#1 2.082(6) Co(2)ϪO(2W) 2.121(7) Co(1)ϪO (21)#2 2.087(6) Co(2)ϪO(1W)#3 2.152(7) Co(1)ϪN (2) 2.154 (8) Co (2) (2) 92.0(3) O(2W)ϪCo (2) phosphonates. [13,14,20] The carboxylateϪ phosphonate ligand is hexadentate and occupies three coordination sites on one Co II ion and also bridges three Co II ions. The phosphonate group containing P (2) is tridentate, whereas the one containing the atom P (1) Figure 2).…”
Section: Resultsmentioning
confidence: 99%