This paper aims at giv ing a practical method for rou tine measu rements of the activ ity of 210 Pb in solids b y gamma spectrometry w ith a w ell G e cry stal. S ince the gamma ray s emitted b y 210 Pb hav e a low energy , 4 6 .5 k eV , the proportion of pu lses cou nted in the cry stal depends strongly on the sample composition trou gh self-attenu ation w ithin the sample itself. S elfattenu ation can b e calcu lated b y u se of a M onte C arlo method b ased on a model. I n the present w ork tw o codes, namely G E AN T 4 and a L ab oratory code gav e resu lts in agreement. H ow ev er, b oth necessitate a good k now ledge of the sample composition, of the detector geometry and of the compu ting programs. I n order to circu mv ent su ch draw b ack s, w as dev eloped an experimental techniq u e, w here the ov erall cou nting efficiency can b e deriv ed directly from the transmission of 4 6 .5 k eV γ−ray s throu gh the sample, b y means of a linear relationship. S u ch correlation w as ob serv ed experimentally w ith samples of k now n activ ity and the approach w as v alidated b y v erification that a linear relation preliminary exists b etw een the transmission and the calcu lated self-ab sorption.