2024
DOI: 10.1021/acs.analchem.4c01110
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Interfacing High-Throughput Electrosynthesis and Mass Spectrometric Analysis of Azines

Krista M. Kulesa,
Erin A. Hirtzel,
Vinh T. Nguyen
et al.

Abstract: Combinatorial electrochemistry has great promise for accelerated reaction screening, organic synthesis, and catalysis. Recently, we described a new high-throughput electrochemistry platform, colloquially named “Legion”. Legion fits the footprint of a 96-well microtiter plate with simultaneous individual control over all 96 electrochemical cells. Here, we demonstrate the versatility of Legion when coupled with high-throughput mass spectrometry (MS) for electrosynthetic product screening and quantitation. Electr… Show more

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