2024
DOI: 10.1002/aic.18421
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Introduced gas regulating fast and highly exothermic reactions with in situ gas generation in microreactors

Saier Liu,
Minjing Shang,
Xiao Xue
et al.

Abstract: The oxidation of cyclohexanol/cyclohexanone with nitric acid as a fast and highly exothermic process was hard to control at low molar ratios of oxidant to organic substrate even in microreactors. Process of runaway gas generation was observed due to the local hot spots, which decreased the selectivity of adipic acid. Additional gas was introduced into microreactors before the reaction, changing the previous wave annular flow to the uniform slug flow. Through the microscopic high‐speed photography and CFD simul… Show more

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