In induction heating processes, knowledge of the charge material parameters, i.e., thermal conductivity and volumetric heat capacity, as well as resistivity and magnetic permeability, is important both at the stage of preparatory process simulations and during their implementation. The paper presents a measurement method for estimating the thermal diffusivity, volumetric heat capacity, and resistivity of the charge material as a function of temperature on a single measuring setup, using a generator for induction heating as the source of signals. The method is based on the study (for forced temperature levels) of the temperature responses of cylindrical samples of the test materials and the voltage induced in the designed measuring coil after short- or long-term step excitation impulses. The presented approach enabled the dedicated computer-controlled system to obtain the initial values of the searched parameters with an accuracy of several percent. The procedure constitutes an introductory step in the simultaneous determination of a set of searched characteristics, and, by performing measurements, significantly narrows the range of variability in the decision variables of the optimization process.