“…TEM analysis exhibit that the newly formed material is a combination of Nano-spherical precipitate and initial phases. The size of nanoparticles (approximately 20 nm [34,35]) and their forms (spherical form) confirm the result obtained by XRD analysis, that the newly formed structure is an amorphous phase. TEM micrographs of MIS based-geopolymer (MISn) and MK based-geopolymer (MKn) don't show any microcracking.…”
“…TEM analysis exhibit that the newly formed material is a combination of Nano-spherical precipitate and initial phases. The size of nanoparticles (approximately 20 nm [34,35]) and their forms (spherical form) confirm the result obtained by XRD analysis, that the newly formed structure is an amorphous phase. TEM micrographs of MIS based-geopolymer (MISn) and MK based-geopolymer (MKn) don't show any microcracking.…”
“…Jia et al [28] found some kind of crack would be existed in the products when the geopolymer was sintered at higher heating rate. But in this experiment, no crack was found at heating rate of 150°C/min.…”
“…In recent years, there has been a growing interest in research concerning development and manufacturing of geopolymer systems with excellent thermal stability at high temperatures [17,18]. In particular, metakaolin and potassium silicate-based geopolymers demonstrated such a properties [19][20][21]. It was reported that dimensional changes are influenced by solid/liquid ratio and related to the kinetics of water release during thermal exposure [22].…”
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