“…have been employed to synthesize RE-doped NaYF 4 material [8][9][10][13][14][15][16][17][18]. Microwave hydrothermal is an improved hydrothermal synthesis approach and increasingly applied in the preparation of micro-/nano-sized materials [17][18][19]. Compared with the conventional hydrothermal method, microwave-assisted hydrothermal has some obvious advantages, such as higher heating rates, shorter reaction time, better controlling of the reaction parameters, higher yields, and excellent reproducibility due to its unique thermal effect induced by microwave heating [19].…”