2010
DOI: 10.1016/j.jallcom.2009.12.084
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Microwave-assisted solid synthesis and impedance spectroscopy of BICRVOX system

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Cited by 14 publications
(5 citation statements)
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“…activation energy observed at low temperature is likely due to trapping of oxygen vacancies at low temperature. This is a classical behaviour for ionic conductors; it is observed for scandia doped zirconia [47,48] and for bismuth based oxide ion conductors, namely BIMEVOX compounds, [49][50][51] too. Although the analysis of impedance diagrams often focuses only on the resistive components, it is also interesting to observe the dependence of the capacitive component as a function of temperature.…”
Section: Electrochemical Characterizationmentioning
confidence: 99%
“…activation energy observed at low temperature is likely due to trapping of oxygen vacancies at low temperature. This is a classical behaviour for ionic conductors; it is observed for scandia doped zirconia [47,48] and for bismuth based oxide ion conductors, namely BIMEVOX compounds, [49][50][51] too. Although the analysis of impedance diagrams often focuses only on the resistive components, it is also interesting to observe the dependence of the capacitive component as a function of temperature.…”
Section: Electrochemical Characterizationmentioning
confidence: 99%
“…As a rapid, simple and effective heating method, microwave irradiation, with direct microwave heating of the molecular precursors, has been widely used in the synthesis of high-quality nanomaterials [34][35][36][37][38][39][40][41][42][43][44][45][46][47][48]. It can reduce the reaction time significantly and has the advantage of uniform heating without heating temperature gradient and lag effect [49][50][51].…”
Section: Introductionmentioning
confidence: 99%
“…It is well known, however, that the prolonged reaction time leads to the increase of crystal sizes. In recent years, the microwave technique has been considered to overcome the above shortcomings [20,21]. The important characteristic of microwave heating is its volumetric effect which results in a much more uniform distribution of heat [22][23][24].…”
Section: Introductionmentioning
confidence: 99%