2018
DOI: 10.1002/tcr.201800121
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Microwave Intensified Synthesis: Batch and Flow Chemistry

Abstract: Many studies have been conducted on organic and inorganic synthesis by microwave heating owing to its special heating mechanism, leading to improved reaction rate, higher purity and yields. We specifically demonstrated microwave heating in the fabrication of nanoparticles and polyester. By fine-tuning the microwave and experimental parameters, the materials prepared have shown excellent physical and bio-properties, e. g. narrow particle size distribution, controlled morphology, varied molecular structure and s… Show more

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Cited by 27 publications
(23 citation statements)
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References 71 publications
(168 reference statements)
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“…Lau et al and Zhang et al discussed another significant advantage of continuous flow reactors over batch reactorsa much greater surface-to-volume ratio. As discussed, the reactants pass through narrow tubes in a continuous flow process whereas they are contained in a flask in a batch process.…”
Section: Influence Of Microwave and Flow Chemistry On Nanoparticle Sy...mentioning
confidence: 99%
“…Lau et al and Zhang et al discussed another significant advantage of continuous flow reactors over batch reactorsa much greater surface-to-volume ratio. As discussed, the reactants pass through narrow tubes in a continuous flow process whereas they are contained in a flask in a batch process.…”
Section: Influence Of Microwave and Flow Chemistry On Nanoparticle Sy...mentioning
confidence: 99%
“…7 In microwave-assisted processes, a large amount of kinetic energy transformed into frictional energy, resulting in the mixing of reactants and heating. 25 It was also seen that within a very short time the temperature of the reactor cavity increased to the optimum level. This resulted in increased methanol evaporation, reducing the potency of the mixture to convert into the bio-diesel.…”
Section: Resultsmentioning
confidence: 94%
“…Recently, continuous MW-assisted flow synthesis of 1,4-dihydropyridines ( 7 ) was achieved using microflow system over γ-Fe 2 O 3 NPs prepared using valve-assisted micromixer ( He et al., 2018 ). Microwave flow systems other than organic synthesis also showed applications in synthesis and fabrication of polyesters and nanoparticles ( Ching Lau et al., 2019 ; Bayazit et al., 2016 ).…”
Section: Importance Of Flow Chemistrymentioning
confidence: 99%