1994
DOI: 10.1016/s0040-4039(00)76988-7
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Model studies towards the insect antifeedant Jodrellin A using an organoselenium mediated cyclization reaction

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Cited by 18 publications
(18 citation statements)
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“…The presence of a C-14,C-15 olefinic double bond in this structural part was revealed by the 1 H-NMR signals at δ 4.79 (1H, t, J 14,13 ) J 14,15 ) 2. 4 Hz, H-14) and 6.45 (1H, t, J 15,13 ) J 15,14 ) 2. 4 Hz, H-15), and the carbon atom resonances at δ 101.8 d (C-14) and 146.9 d (C-15).…”
Section: Resultsmentioning
confidence: 99%
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“…The presence of a C-14,C-15 olefinic double bond in this structural part was revealed by the 1 H-NMR signals at δ 4.79 (1H, t, J 14,13 ) J 14,15 ) 2. 4 Hz, H-14) and 6.45 (1H, t, J 15,13 ) J 15,14 ) 2. 4 Hz, H-15), and the carbon atom resonances at δ 101.8 d (C-14) and 146.9 d (C-15).…”
Section: Resultsmentioning
confidence: 99%
“…4 Hz, H-14) and 6.45 (1H, t, J 15,13 ) J 15,14 ) 2. 4 Hz, H-15), and the carbon atom resonances at δ 101.8 d (C-14) and 146.9 d (C-15). (See Tables 1 and 2 for the remaining proton and carbon resonances of the C-11-C-16 fragment).…”
Section: Resultsmentioning
confidence: 99%
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“…16 For the majority of the preceding transformations, NPSP has been found the superior reagent both in terms of chemical efficiency as well as the mild nature of the reaction conditions that are typically employed. 17 MeO 27 and thioesters 28 (as in eqs 6, 7, 9, and 14) have been reported, along with new instances where NPSP was utilized for the conversion of alcohols to selenides 29 (as in eq 15) and carboxylic acids to selenoesters 30 (as in eq 16). Several new applications of NPSP, as well as recent variations of the above processes, are described below.…”
Section: Avoid Skin Contact With All Reagentsmentioning
confidence: 98%